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' 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCA vIPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax: 925-798-1622 <br />' httu://www.mccampbell.com E-mail:main@mccampbell.com <br />' <br /> Date Sampled: 09/30/99 <br /> Advanced GeoEnvironmental Client Project ID: Geweke <br /> Date Received: 10/02/99 <br /> 4005 North Wilson Way <br />' Stockton,CA 95205 Client Contact:Kevin McKibben Date Extracted: 10107-10/12/99 <br /> Client P.O: Date Analyzed: 10/07-10/12/99 <br />' Volatile Organics By GCIMS <br /> EPA method$260 <br /> Lab ID 22677 <br />' Client ID M W 14 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone°r ND<5 trans-l,3-Dichloropropene ND <br />' Benzene 6.9 Ethylene dibromide ND <br /> Bromobenzene ND E.thyibenzene 3.2 <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND lodomethane ND <br />' Bromoform ND Isopropylbenzene 1.8 <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone ND <br /> sec-Bucy]benzene ND Methylene Chloride"' ND <br />' tert-Butyl benzene ND Methyl ethyl ketone ND <br /> Carbon Disulfide ND Methyl isobutyl ketone ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND Naphthalene ND <br /> lie Chloroethane ND n-Propyl benzene 1.6 <br /> 2-Chloroethyl Vinyl Ether` ND Styrene ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene m 5.4 <br /> Dibromochloromethane ND 1,2,3-Trieblorobenzene ND <br /> 1,2-Dibromo-3-chloropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> I 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> 1,1-Dichloroethane ND 1,2,4-Trimethylbenzene 11 <br /> 1,2-Di chloroethane 27 1,3,5-Trimethylbenzene 2.7 <br /> I 1,1-Dichloroethene ND Vinyl Acetate 22 <br /> cis-1,2-Dichloroethene ND Vinyl ChlorideND <br /> trans-l,2-Dichloroethene ND Xylenes,total 39 <br /> 1,2-Dichloropropane ND Comments: <br /> I 1,3-Dichloropropane ND Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 120 <br /> 1,1-Dichloropropene ND Toluene-d8 100 <br /> cis-1,3-Dichloropropene ND 4-Bromofluorobenzene 95 <br /> -water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples I ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> I ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (e) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2 <br /> . pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than —5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br />' chloroethene;(0)dimethylbenzenes. <br /> DHS Certification No. 1644Edward Hamilton, Lab Director <br />