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I110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax :925-798-1622 <br /> /www lJ&g E-mail:main@mccampbell.com <br /> I <br /> Advanced GeoEnviromnental Client Project ID: Geweke Date Sampled: 03/17/99 <br /> 4005 North Wilson Way <br /> Date Received: 03/19/99 <br /> Stockton, CA 95205 Client Contact:Kevin McKibben Date Extracted: 03/21-03/24/99 <br /> IClient P.O: Date Analyzed: 03121-03/24/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 05366 <br /> Client ID MW-8 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<6 Ethylbenzene 81 <br />' Benzene ND<3.3 Hexachlorobutadiene ND<3.3 <br /> Bromobenzene ND<3.3 Iodomethane ND<3.3 <br /> Bromochloromethane ND<3.3 lsopropylbenzene 35 <br /> Bromodichloromethane ND<3.3 p-Isopropyl toluene 5.1 <br /> Bromoform ND<3.3 Methyl butyl ketone ND<3.3 <br /> Brornomethane ND<3.3 Methylene Chloride` ND<3.3 <br /> n-Butyl benzene ND<3.3 Methyl ethyl ketone ND<3.3 <br /> sec-Butyl benzene 5.8 Methyl isobutyl ketone a ND<3.3 <br /> lent-Butyl benzene ND<3.3 Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND<3.3 Napthalene ND<3.3 <br /> Carbon Tetrachloride NDX3.3 n-Propyl benzene ND<3.3 <br /> Chlorobenzcne ND<3.3 Styrene ND<3.3 <br /> Chloroethane ND<3.3 3,3,1,2-Tetrachloroeth2ne ND<3.3 <br /> 2-Chloroethyl Vinyl Ethe ND<3.3 1,1,2,2-Tetrachloroethane ND<3.3 <br /> Chloroform ND<3.3 Tetrachloroethene ND<3.3 <br /> Chloromethane NIK3.3 Toluene ND<3.3 <br /> 2-Chlorotoluene ND<3.3 1,2,3-Trichlorobenzene ND<3.3 <br /> 4-Chlorotoluene ND<3.3 1,2,4-Trichlorobenzene ND<3.3 <br /> Dibromochloromethane ND<3.3 1,1,1-Trichloroethane ND<3.3 <br /> 1,2-Dibromo-3-chloropropane NIx3.3 1,1,2-Trichloroethane ND<3.3 <br /> Dibromomethane ND<3.3 Trichloroethene ND<3.3 <br /> 1,2-Dichlorobenzene ND<3.3 Trichlorofluoromethane ND<3.3 <br /> 1,3-Dichlorobenzene ND<3.3 1,2,3-Trichl oropropane ND<3.3 <br /> I 1,4-Dichlorobenzene N13<3.3 1,2,4-Trimethylbenzene 140 <br /> Dichlorodifluoromethane ND<3.3 1,3,5-Trimethylbenzene 48 <br /> I,l-Dichloroethane ND<3.3 Vinyl Acetate"' ND<3.3 <br /> 1,2-Dichloroethane 9.7 Vinyl Chloride ND<3.3 <br /> 1,1-Dichloroethene ND<3.3 Xylenes,total '° 57 <br /> cis-1,2-Dichloroethene ND<3.3 <br /> trans-1,2-Dichloroethene ND<3.3 <br /> 1,2-Dichloropropane ND<3.3 <br /> I 1,3-Dichloropropane ND<3.3 <br /> 2,2-Dichloropropane ND<3.3 Comments:j <br /> 1,1-Diehl oropropene N13<3.3 Surrogate Recoveries <br /> cis-1,3-Dichloropropene ND<3.3 Dibromofluoromethane 92 <br /> trans-I,3-Dichloropropene ND<3.3 Toluene-d8 107. <br /> Ethylene dibromide ND<3.3 4-Bromofluorobenzene 96 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ughi&*and all TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-prop2none or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> . pentanone or isopropyiacetone; (h)lighter than water immiscible sheen is present; (i) liquid sample that contains greater than -5 vol. % <br /> I sediment;6)sample diluted due to high organic content; (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />