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' 110 Second Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax:925-798-1622 <br /> hltF:/lwww.mccamphell.com E-mail:main@mccampbell.com <br /> • Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 03/17/99 <br /> 4005 North Wilson Way Date Received: 03/19/99 <br /> Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 03/21-03/24199 <br />' Client P.O: Date Analyzed: 03/21-03/24199 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 05368 <br /> Client ID MW-10 <br />' Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone' ND<3 Ethylbenzene ND <br />' Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND Iodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br />' Bromoform ND Methyl butyl ketone ND <br /> Bromomethane ND Methylene Chloride"' ND <br /> n-Butyl benzene ND Methyl ethyl ketone` ND <br />' sec-Butyl benzene ND Methyl isoburyl ketone a ND <br /> tert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) <br /> Carbon Disulfide ND Naptbalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br />' Chlorobenzene ND Styrene ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether" ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethane ND <br /> Chloromethane ND Toluene ND <br /> 2-Chlorotoluene ND 1,2,3-Trichlorobenzene ND <br /> 4-Chlorotoluene ND 1.2,4-Trichlorobenzene ND <br /> Dibromochloromethane ND 1,1,3-Trichloroethane ND <br /> I <br /> 1,2-Dibromo-3-chi oropropane ND 1,1,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Trichloropropane ND <br />' 1,4-Dichlorobenzene ND 1,2,4-Tri methylbenzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Trimethylbenzene ND <br /> 1,1-Dichloroethane ND Vinyl Acetate'"' ND <br /> 1,2-Dichloroethane ND Vinyl Chloride " ND <br /> 1,1-Dichloroethene ND Xylenes,total ° ND <br /> cis-1,2-Dichloroethene ND <br /> trans-3 2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> I 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments: <br /> 3,1-Dichloropropene ND Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND Dibromofluoromethane 94 <br />' trans-1,3-Dichloropropene ND Toluene-d8 124. <br /> Ethylene dibromide ND 4-13romofluorobenzene 109 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than --5 vol. % <br /> sediment;0)sample diluted due to high organic content; (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethane;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 /V Edward Hamilton,Lab Director <br />