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' 110 2nd Avenue South,#1)7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone : 925-798-1620 Fax :925-798-1622 <br /> ://www,mccaml2bell.cgm E-mail: main@mccampbell.com <br /> iAdvanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 06/24/99 <br /> 4005 North Wilson Way Date Received: 06/28/99 <br />' Stockton, CA 95205 Client Contact:Kevin McKibben Date Extracted: 06/28-07/06199 <br /> Client P.O: Date Analyzed: 06128-07/06/99 <br />' EPA method 8260 Volatile Organics By GC/MS <br /> Lab ID 14474 <br />' Client ID MW-6/6-24-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<5 trans-1,3-Dichioropropene ND <br />' Benzene ND Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND Iodomethane ND <br /> I Bromoform ND lsopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone" ND <br /> sec-Butyl benzene ND Methylene Chloride"' ND <br />' tert-Butyl benzene ND Methyl ethyl ketone-'T- ND <br /> Carbon Disulfide ND Methyl isobutyl ketones ND <br /> Carbon Tetrachloride ND Methyl tert-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-ChloroethylVinyl Ethe ° ND Styrene"I ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorwoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene" ND <br /> Dibromochloromethane ND 1,2,3-Trichlorobenzene ND <br /> I 1,2-Dibmmo-3-chloropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> I 1,4-Dichloroben7ene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Tri chi oropropane ND <br /> I,l-Dichloroethane ND 1,2,4-Trimethyiben2ene ND <br /> 1,2-Dichloroethane ND 1,3,5-Trimethylbenzene ND <br /> 1,1-Dichloroethene ND Vinyl Acetate " ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride'°' ND <br /> trans-1,2-Dichloroethene ND Xylenes,total ND <br /> 1,2-Dichloropropane ND Comments: <br /> 1,3-Dichloropropane ND Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND Dibromofluoromethane <br /> 1,1-Dichloropropene ND Toluene-d8 103 <br /> cis-1,3-Dichloropropene ND 4-Bromofluorobenzene 113 <br /> 'Reporting <br /> and vapor samples are reported in ug/L,soil and sludge samples in uglkg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples I ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> I (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hex2none; (e) dichloromethane; (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present (i) liquid sample that contains greater than --5 vol. % <br /> sediment; (j) samp]e diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> ch]oroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 . Edward Hamilton, Lab Director <br /> I <br />