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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> httn://www.mcca bell.com E-mail:main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 06/24/99 <br /> 4005 North Wilson Way Date Received: 06/28/99 <br />' Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 06/28-07/06/99 <br /> Client P.O: Date Analyzed:06/28-07/06/99 <br />' EPA method 8260 Volatile Organics By GC/MS <br /> Lab ID 14480 <br />' Client ID MW-14/6-24-99 <br /> Matrix W <br /> Compound Concentration* Com ound Concentration* <br /> Acetone(b) ND trans-l,3-Di chloropropene ND <br /> Benzene 6.2 Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene 5.4 <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND lodomethane ND <br />' Bromoform ND lsopropylbenzene 1.5 <br /> Bromomethane ND ..2-Isopropyl toluene ND <br /> n-Butyl benzene 1.0 Methyl butyl ketone' ) ND <br /> see-Butyl benzene 1.3 Methylene Chloride" ND <br /> Cert-Butyl benzene ND Methyl ethyl ketone 16 ND <br /> Carbon Disulfide ND Methyl isobutyl ketone(61 ND <br /> Carbon Tetrachloride ND Methyl ten-Butyl Ether(MTBE) __- <br /> Chlorobenzene ND Na hthalene ND<3 <br /> Chloroethane ND n-Propyl benzene 1.0 <br /> 2-Chloroethyl Vinyl Ether`) ND Styrene(') ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene"° 14 <br /> Dibromochloromethane ND 1,2,3-Trichlorobenzene ND <br /> I 1,2-Dibromo-3-chloropro ane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND I,1,]-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> I,1-Dichloroethane ND 1,2,4-Trimethylbenzene I! <br /> 1,2-Dichloroethane 32 1,3,5-Trimethylbenzene 5.4 <br /> 1,1-Dichloroethene ND Vinyl Acetate'") 5.8 <br /> cis-1,2-Dichloroethene ND Vinyl Chloride`O) ND <br /> trans-l,2-Dichloroethene ND Xylenes,total `P' 55 <br /> 1,2-Dichloro ropane ND Comments: <br /> I 1 3-Dichloro ro ane ND Surrogate Recoveries <br /> 2,2-Dichloropropane ND Dibromofluoromethane 95 <br /> ],!-Dichloropropene ND Toluene-dS 96 <br /> cis-1,3-Dichloro ro ene ND 4-Bromofluorobenzene 105 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropyl acetone; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. % <br /> sediment; 6) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene; o dimeth 9benzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />