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r <br /> t> I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax :925-798-1622 <br /> http://www.mccaml2bcll.gg E-mail:main@mccampbell.com <br /> • <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 09/10/98 <br /> 4005 North Wilson Way <br /> Date Received: 09/11/98 <br /> Stockton,CA 95205 Client Contact: Kevin McKibben Date Extracted: 09/11-09/15/99 <br /> Client P.O: Date Analyzed: 09/11-09/15/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 94790 <br /> Client ID MW8/9-10-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> AcetoneND<5 Ethylbenzene 160 <br /> Benzene 8.6 Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND I sopropy]benzene 25 <br /> Bromodichloromethane ND p-Isopropyl toluene 2.2 <br /> Bromoform ND Methyl butyl ketone` ND <br /> Bromomethane ND Methylene Chloride ' ND <br /> n-Butyl benzene 8.1 Methyl ethyl ketone"' ND <br /> sec-Butyl benzene 3.6 Methyl isobutyl ketone's ND <br /> tert-Butyl benzene ND Methyl cert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND Naphthalene NDc30 <br /> Carbon Tetrachloride ND n-Propyl benzene 50 <br /> Chlorobenzene ND Styrene ' ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether"' ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> Chloromethane ND Toluene" ND <br /> 2-Chlorotoluene ND 1,2,3-Trichlorobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Triehlorobenzene ND <br /> Dibromochloromethane ND 1.1,1-Trichloroethane ND <br /> 42-Dibromo-3-chloropropane ND 1,1,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Trichloropropane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Trimethylbenzene 320 <br /> Dichlorodifluoromethane ND 1,3,5-Trimethylbenzene 30 <br /> 1,1-Dichloroethane ND Vinyl Acetate""' 8.3 <br /> 1,2-Dichloroethane 7.0 Vinyl Chloride"' ND <br /> 1,1-Dichloroethene ND Xylenes,total '° 110 <br /> cis-1,2-Dichloroethene ND <br /> trans-1,2-Dichloroethene ND <br /> 1,2-Dicltloropropane ND <br /> 1,3-Dichloropmpane ND <br /> 2,2-Dichloropropane ND Comments: <br /> 1,1-Dichloropropene ND Surrogate Recoveries('%P) <br /> cis-1,3-Dichloropropene ND Dibromotluoromethane 100 <br /> trans-1,3-Dichloropropene ND Toluene-d8 99 <br /> Ethylene dibromide ND 4-13romotluombenzene 95 <br /> water and vapor samples are reported in ug/l-.,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2uglwipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone, (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than —5 vol. % <br /> sediment;O sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroetbene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />