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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone;925-798-1620 Fax :925-798-1622 <br /> http://www.mccampbell.com E-mail: main@mccampbell.com <br /> iDate Sampled: 12/21/98 <br /> Advanced GeoEnvirortmental Client Project ID: Geweke <br /> Date Received: 12/22/98 <br /> 4005 North Wilson Way <br /> Client Contact: Kevin McKibben Date Extracted:01102-01105199 <br /> Stockton, CA 95205 I <br /> Client P.O: Date Analyzed:01/02-01105199 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 00790 <br /> Client ID MW-14112-21-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone" ND<5 Ethylbenzene ND<3 <br /> Benzene ND<3 Hexachlorobutadiene ND<3 <br /> Bromobenzene ND<3 lodomethane ND<3 <br /> Bromochloromethane ND<3 1 sopropylbenzene ND<3 <br /> Bromodichlommethane ND<3 p-Isopropyl toluene ND<3 <br /> Bromoform ND<3 Methyl butyl ketone` ND<3 <br /> Bromomethane ND<3 Methylene Chloride"' ND<3 <br /> n-Butyl benzene ND<3 Methyl ethyl ketone" ND<3 <br /> sec-Butyl benzene ND<3 Methyl isobutyl ketone'$ ND<3 <br /> tert-Butyl benzene ND<3 Methyl cert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<3 Napthalene ND<3 <br /> Carbon Tetrachloride ND<3 n-Propyl benzene ND<3 <br /> Chlorobenzene ND<3 Styrene" NDV <br /> Cbloroethane ND<3 1,1,1,2-Tetrachloroethane ND<3 <br /> 2-Chloroethyl Vinyl Ether` ND<3 3,1,2,2-Tetrachloroethane ND<3 <br /> Chloroform ND<3 Tetrachloroethene ND<3 <br /> Chloromethane ND<3 Toluene ND<3 <br /> 2-0110rotol uene ND<3 1,2,3-Trichl orobenzene ND<3 <br /> 4-Chlorotoluene ND<3 1,2,4-Trichlorobenzene 3.6 <br /> Dibromochloromethane ND<3 1,1,1-Trichloroethane ND<3 <br /> 1,2-Dibromo-3-chlor0pr0p2ne ND<3 1,1,2-Trichloroethane ND<3 <br /> Dibromomethane ND<3 Trichloroethene ND<3 <br /> 1,2-Dichlorobenzene ND<3 Trichlorofluoromethane ND<3 <br /> 1,3-Dichlorobenzene ND<3 1,2,3-Trichloropropane ND<3 <br /> 1,4-Dichlorobenzene ND<3 1,2,4-TTimethylbenzene N D<3 <br /> Dichlorodifluoromethane ND<3 1,3,5-Trimethylbenzene ND<3 <br /> IJ-Dichloroethane ND<3 Vinyl Acetate" 4.8 <br /> 1,2-Dichloroethane 50 Vinyl Chloride" ND<3 <br /> ],1-Dichloroethene ND<3 Xylenes,total 15 <br /> cis-1,2-Dich loroethene ND<3 <br /> trans-1,2-Diehl oroethene ND<3 <br /> 1,2-Dichloropropane ND<3 <br /> 1,3-Dichloropropane ND<3 <br /> 2,2-Dichloropropane ND<3 Comments: <br /> 1,1-Dichioropropene ND<3 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<3 Dibromofluoromethane 103 <br /> trans-l,3-Di chioropropene ND<3 Toluene-d8 98 <br /> Ethylene dibromide ND<3 4-Bromofluorobenzene 92 <br /> -water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than --5 vol. % <br /> sediment;0)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 %1 Edward Hamilton, Lab Director <br />