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1102nd Avenue South #D7 Pacheco,CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br /> Website www mecampbOl corn Email nwin@mc campb0J loin <br /> Advanced GeoEnvironmental, Inc Client Project ID Geweke Date Sampled 09/09/04 <br /> 837 Shaw Road Date Received 09/10/04 <br /> Stockton,CA 95215 Client Contact Bob Marty Date Extracted 09/10/04-09111104 <br /> Client P O Date Analyzed 09/10/04-09/11104 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GCIMS* <br /> ExtracuonMethod SW5030B Ana Method SW8260B Work Order 0409135 <br /> Lab ID 0409135-005B 0409135-006B 10409135-007B 0409135-008B <br /> Client ID M W 12 MW 14 MW t 5 I MW 16 Reporting Limit for <br /> Matrix W W W W DF=1 <br /> DF I 1 1 I S W <br /> Compound Concentration ug/kg ug/L <br /> tert-Amyl methyl ether(TAME) NO ND ND NO NA 05 <br /> t-Butyl alcohol(TBA) NO 72 ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) NO NO ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) NO 7 l NO 56 NA 05 <br /> Dusopropyl ether(DEPE) ND ND ND NO NA 05 <br /> Ethyl tert-butyl ether(ETBE) NO NO NO NO NA 05 <br /> Methyl-t-butyl ether(MTBE) NO NO NO NO NA 05 <br /> Surrogate Recoveries(%) <br /> %SS 93 5 88 8 892 845 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLA extracts are reported toµg/L,soil/sludge/solid samples inµg/kg, wipe samples in Ag/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> NO means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate c,oelutes with another peak <br /> L"h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--1 vol %sediment,j)sample diluted due to high <br /> or ante content <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />