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110 2nd Avenue South #D7 Pacheco CA 94553 5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> http/lwww mccampbell corn F rnmil mam meta bell cam <br /> Advanced GeoEnvironmental, Inc Client Project ID Geneke Date Sampled 09/10/03 <br /> 837 Shaw Road Date Received 09/11/03 <br /> Stockton,CA 95215 Client Contact Brian Millman Date Extracted 09113/03-09117/03 <br /> Client P O Date Analyzed 09113103-09/17/03 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Atialytical Method SW8260B Work Order 0309193 <br /> Lab ID 0309193-005B 0309193-006B 0309193-0078 0309193-0088 <br /> Client ID MW 14 MW 15 MW 16 MW 17 Reporting Limit for <br /> Matrix --W ---- Wrn�- ——W - - '----—W ---- DF=l <br /> DF 1 1 1 1 S pr <br /> Compound Concentration ug/kg pg/L <br /> Dnsopropyl ether(D1PE) ND ND ND ND NA 05 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND NA 05 <br /> Methyl-t-butyl ether(MTBE) ND I ND ND ND NA 05 <br /> tert-Amyl methyl ether(TAME) ND ND ND ND NA 05 <br /> t-Butyl alcohol(TBA) 99 ND ND ND NA 50 <br /> 1,2-Dibromoethane(EDB) ND ND ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) 20 ND 22 ND NA 05 <br /> Surrogate Recoveries(%) <br /> 108 105 108 <br /> Comments E I - -I <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in AWL,so,Usludgelsolid samples in gg/kg, wipe samples in pg/wipe <br /> product/oil/non-aqueous liquid samples to mglL <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> ##surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheeniproduct is present,i)liquid sample that contains greater than—2 vol %sediment,1)sample diluted due to high <br /> organic content <br /> I <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />