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I <br /> 1 10 Second Avenue South,#tD7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 510-798-1620 Fax : 510-798-1622 <br />' 44 http:/hvww.niecampbell.com E-mail:main@rnecampbell.com <br />' Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 12/16/97 <br /> 4005 North Wilson Way Date Received: 12/18/97 <br />' Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 12/20-12/22/97 <br /> Client R.O: Date Analyzed: 12120-12/22/97 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 84300 <br />' Client ID MW-7/12-16-97 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br />' Acetone' ' ND Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br />' Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl keloneND <br /> Bromomethane ND Methylene Chloride"' ND <br />' n-Butyl benzene ND Mctllyl ethyl ketone' ' ND <br /> sec-Butyl benzene ND Methyl isobutyl ketone'E ND <br /> tert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) ND <br /> Carbon Disulfide ND Naphthalene ND <br /> 10 Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene' ' LID <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether" ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroetheoe ND <br /> Chloromethane ND Toluene" ND <br /> 2-Chlorotoluene ND 1,23-Tricklorobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Trichlorobenzene ND <br />' Dibromochloromethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichkn-othEoromethane ND <br />' 1,3-Dichlorobenzene ND 1,2,3-Trichloropropane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Trimethylbenzene ND <br /> Dichlorodifluoromethane ND i,3,5-Trimethy)benzene ND <br /> 1,1-Dichloroethane ND Vinyl Acetate""' ND <br />' 1,2-Dichloroethane ND Vinyl Chloride"" ND <br /> ],1-Di chloroethene ND aylenes,total "" ND <br /> cis-1,2-Dichloroethene ND TPH-(g)(Co-C'12) --- <br /> trans-1,2-Dichloroethene ND TPH-(ms)(C'8-('12) -- <br />' 1,2-Dichloropropane ND TPH-(k)((-10+) --- <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments: <br /> l,1-Dichloropropene ND Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND Dibrom0111.1oromethane 100 <br /> trans-1,3-Dichloropropene ND Toluene-d8 102 <br /> Ethylene dibromide ND 4-Bromo[luorobenzene 95 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 0.5 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> . 0.2ug/wipe ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2.propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. % <br /> sediment;0)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 -Edward Hamilton, Lab Director <br />