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I <br /> I 10 Second Avenue South,#✓137,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Telephone : 510-798-1620 Fax : 510-798-1622 <br />' http://wu,a,.niceampbell.com E-mail:main@mccampbell.com <br /> • <br /> IAdvanced GeoEnvironmental Client Project 1D: Geweke Date Sampled: 12/16/97 <br /> 4005 North Wilson Way <br /> Date Received: 12/18/97 <br />' Stockton, CA 95205 Client Contact:Kevin McKibben Date Extractdd: 12120-12/22/97 <br /> Client P.O: Date Analyzed: 12120-12122197 <br /> iVolatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 54302 <br />' Client 1D lv1Vt'-9112-16-97 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone" ND<3 Ethylbenzene 39 <br /> Benzene 4.0 Hexachlorobutadiene ND<3 <br /> Bromobenzene ND<3 lodomethane ND<3 <br />' Bromochloromethane ND<3 lsopropylbenzcne 14 <br /> BrOmodichloromelhane ND<3 p-Isopropylloluene ND<3 <br /> Bromoform ND<3 Methyl butyl ketone' ' ND<3 <br /> Bromomethane ND<3 Methylene Chloride"' NIX3 <br /> n-Butyl benzene 5.3 Methyl ethyl ketone"I ND<3 <br /> sec-Butyl benzene 7.1 Methyl isobutyl ketoneND<3 <br /> tent-Butyl benzene ND<3 Metbyi tert-Butyl Ether(Ml'BE) ND<3 <br /> Carbon Disulfide ND<3 Naphthalene 5.7 <br /> lieCarbon Tetrachloride ND<3 n-Propyl benzene 15 <br /> Chlorobenzene ND<3 Styrene' ' ND<3 <br /> Chforoethane ND<3 1,1,1,2-Tetrachloroethane ND<3 <br /> 2-Cltloroethyl Vinyl Ether"' ND<3 1,1.2,2-Telmchloroethane ND<3 <br /> Chloroform ND<3 Tetrachloroethene ND<3 <br /> Chloromethane ND<3 Toluene"' 4.2 <br /> 2-Chlorotoluene ND<3 1,2,3-Trichlorobenzene ND<3 <br /> 4-Chlorotol u ene ND<3 12,4-Trichlorobenzene ND<3 <br /> Dibromochloromethane ND<3 1,1,1-Trichloroethane ND<3 <br /> 1,2-Dibromo-3-chloropropane ND<3 1,1.2-Trichloroethane ND<3 <br /> Dibromomethane ND<3 Trichloroethene ND<3 <br /> 1,2-Dichlorobenzene ND<3 Trichlorofluoromethane ND<3 <br /> 1,3-Dichlorobenzene ND<3 1.2,3-Trichlompropane ND<3 <br /> 1,4-Dichlorobenzene ND<3 1,2,4-Trimethylhenzene 50 <br /> Dichlorodifluoromethane ND<3 1.3.5-Trimethylbenzenc 15 <br /> ],I-Dichioroethane ND<3 Vinyl Acetate""' 2.9 <br /> 1,2-Dichloroethane 20 Vinyl Chloride"" ND<3 <br /> 1,1-Dichloroethene ND<3 Xylenes,total "" 29 <br /> cis-1,2-Di chloroethene ND<3 TPH-(g)(Co-C'l2) --- <br /> trans-1,2-Dichloroethene ND<3 TPH-(nts)(C'S-(-'12) --- <br /> 1,2-Dichloropropane ND<3 TPH-(k)(C10+) --- <br /> 1,3-Dichloropropane ND<3 <br /> 2,2-Dichloropropane ND<3 Comments: <br /> I 1,1-Dichloropropene NIX3 Sorvogulte Recoveries(%) <br /> cis-1,3-Dichloropropene ND<3 Dibromotluorometltane ]01 <br /> trans-l,3-Di chloropropene ND<3 Toluene-d8 107 <br /> Ethylene dibromide ND<3 4-Brontofluorobenzene 102 <br /> I "water and vapor samples arereported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 0.5 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> I pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present: (i) liquid sample that contains greater than —5 vol. % <br /> sediment;0)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;(o) imcl! (benzenes. <br /> IDHS Certification No. 1644 Edward Hamilton,Lab Director <br /> I <br />