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110 Second Avenue South,OD7,Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC. Telephone : 510-798-1620 Fax :510-798-1622 <br />' http://w,,vw.mccampbell.cotn E-mail: main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project 1D: Geweke Date Sampled: 12/16/97 <br /> 4005 North Wilson Way Date Received: 12/18/97 <br />' Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 12/20-12/22/97 <br /> Client P.O: Date Analyzed: 12/20-12/22/97 <br />' Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 84305 <br />' Client ID M\V-14/12-16-97 <br /> Matrix w <br /> Compound Concentration* Cotttpottnd Concentration* <br />' Acetone" ND<10 Ethylbenzene 51 <br /> Benzene 130 Hexachlorobutadiene ND<10 <br /> Bromobenzene ND<10 lodomethane ND<10 <br /> Bromochloromethane ND<10 Isopropylbenzene ND<10 <br />' Bromodichloromethane ND<10 p-Isopropyl toluene ND<10 <br /> Bromoform N0<10 Methyl butyl ketone' ' NEXi0 <br /> Bromomethane ND<10 Methylene Chloride'" ND<10 <br />' n-Butyl benzene ND<10 Methyl cthyl lketoae' ' ND<10 <br /> sec-Butyl benzene ND<10 Methy)isobutyl ketone'F ND<10 <br /> tent-Butyl benzene ND<10 Methyl tert-Butyl Fther(MTBE) ND<10 <br /> Carbon Disulfide ND<10 Naphthalene NEX10 <br /> Carbon Tetrachloride ND<l0 n-Propyl benzene ND<10 <br /> Chlorobenzene ND<10 Styrene` ' ND<10 <br /> Chloroethane ND<10 1,1,1,2-Tetrachloroethane ND<l0 <br /> 2-Chloroethyl Vinyl Ether" ND<10 1,1.2,2-Tetrachloroethane ND<10 <br /> Chloroform ND<10 Tetrachloroethene ND<10 <br /> Chloromethane ND<10 Toluene" 98 <br /> 2-Chlorotoluene ND<10 1.2.3-Trichlorobenzene ND<10 <br /> 4-Chlorotoluene ND<10 l,2,4-Trichlorobenzene ND<10 <br />' Dibromochloromethane ND<10 1,1,1-Trichloroohane ND<10 <br /> 1,2-Dibromo-3-chloropropane ND<10 1,1,2-1-richloroethane ND<10 <br /> Dibrornomethane ND<10 Trichloroethene ND<10 <br /> 1,2-Dichlorobenzene ND<10 Ti'iclllorolliioi-l}nleSliane ND<10 <br /> 1,3-Dichlorobenzene ND<10 l,2,3-Trichloropropane ND<10 <br /> 1,4-Dichlorobenzene ND<10 1,2,4-l-rimethylbenzene 74 <br /> Dichlorodifluoromethane ND<10 1.3.5-Trimethyihenzene 17 <br /> l,l-Di chloroethane ND<10 Vinyl Acetate""' 11 <br />' <br /> 1,2-Dichloroethane 37 Vinyl C.'hloride'"' ND<10 <br /> 1,1-Dichloroethene ND<10 Xylenes,total ." 260 <br /> cis-1,2-Dichloroethene ND<10 TPH-(g)(C6-C'32) <br /> trans-1,2-Dichloroethene ND<10 TPH-(ms)(C'8-C12) -- <br />' 1,2-Dichloropropane ND<10 TPH-(k)(C10+) --- <br /> 1,3-Dichloropropane ND<10 <br /> 2,2-Dichloropropane ND<10 Comments: <br /> 1,1-Dichloropropene ND<10 Surrogate Recoveries('%) <br />' cis-1,3-Dich3oropropene ND<10 DibromotluorOTIMhanc 98 <br /> trans-l,3-Dichloropropene ND<10 Toluene-d8 102 <br /> Ethylene dibromide ND<10 4-Bromotluorobenzene 99 <br />' 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,U ipe,in oglwipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 0.5 uglL; vapor samples 11.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hex3none; (e) dtchlorotnethane; (f) 2-butanone; (g) 4-methyl-2- <br />' pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present. (i)liquid sample that contains greater than —5 vol. % <br /> sediment;(.I)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern o£our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroelhene;(n)dimethylhenzenes. <br /> DHS Certification No. 1644 ✓Edward Hamilton, Lab Director <br /> I <br />