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I 10 Second Avenue South,#D7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Telephone: 510-798-1620 Fax : 510-798-1622 <br /> http://Nvww.n)ccanipbell.com E-mail: main@mccampbell.com <br /> • <br /> Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 09/16/97 <br /> 1803 West March Lane,Ste A Date Received: 09/17/97 <br /> Stockton, CA 95207 Client Contact: Kevin McKibben Date Extracted: 09/20/97 <br /> Client P.O: Date Analyzed: 09/20/97 <br /> Volatile Organics By GC/117S <br /> EPA method 8260 <br /> Lab ID 80838 <br /> Client ID MW-14/9-16-97 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone' ND<20 trans-1,3-Dichloropropene ND<20 <br /> Benzene 240 Ethylene dibromide' ' ND<20 <br /> Bromobenzene ND<20 Ethylbenzene 85 <br /> Bromochloromethane ND<20 Hexachlorobutadiene ND<20 <br /> Bromodichloromethane ND<20 lodomethane ND<20 <br /> Bromoform ND<20 Isopropylbenzene ND<20 <br /> BTOmOmethane ND<20 p-Isopropyl toluene ND<20 <br /> n-Butyl benzene ND<20 Methyl butyl ketone"' ND<20 <br /> sec-Butyl benzene ND<20 Methylene Chloride"' ND<20 <br /> tert-Butyl benzene ND<20 Methyl ethyl ketone'' ND<20 <br /> Carbon Disulfide ND<20 Methyl isobutyl ketone' ' ND<20 <br /> Carbon Tetrachloride ND<20 Methyl Cert-Butyl Ether(NITBE) --- <br /> Chlorobenzene ND<20 Napthalene ND<20 <br /> Chloroethane ND<20 n-Propyl benzene ND<20 <br /> 2-Chloroethyl Vinyl Ether" ND<20 Styrene` ND<20 <br /> Chloroform ND<20 1,1,1,2-Tetrachloroethow ND<20 <br /> Chloromethane ND<20 1,1,2,2-Tetrachloroethane ND<20 <br /> 2-Chlorotoluene ND<20 Tetra chloroethene ND<20 <br /> 4-Chlorotoluene ND<20 Toluene""' 170 <br /> Dibromochloromethane ND<20 1.2.3-Trichlorobenzene ND<20 <br /> 1,2-Dibromo-3-chloropmpane ND<20 1,2,4-Trichlorobenzene ND<20 <br /> Dibromomethane ND<20 1,1,1-Trichloroethane ND<20 <br /> 1,2-Dichlorobenzene ND<20 1,1,2-Trichloroethane ND<20 <br /> 1,3-Dichlorobenzene ND<20 Trichloroethene NID<20 <br /> 1,4-Dichlorobenzene ND<20 Trichlorotluoromet},ane ND<20 <br /> Diehl orodilluoromethane ND<20 1,23-Trichloropropanc ND<20 <br /> ],l-Dichloroethane ND<20 ],2,4-Tdmethylbenzene 110 <br /> 1,2-Dichloroethane ND<20 1,3,5-Trimethylbenzene 20 <br /> ],l-Dichloroethene ND<20 Vinyl Acetate"" ND<20 <br /> cis-1,2-Dichloroethene ND<20 Vinyl Chloride`O1 ND<20 <br /> trans-1,2-Dichloroethene ND<20 Xylenes,total ''" 460 <br /> 1,2-Dichloropropane ND<20 Comments: <br /> 1,3-Dichloropropane ND<20 Surrogate Recoveries(1A) <br /> 2,2-Dichloropropane ND<20 Dibromolluoromethane 107 <br /> 1,1-Dichloropropene ND<20 Toluene-d8 96 <br /> cis-1,3-Dichloropropene ND<20 4-Bromotluorobenzene 91 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L:solid and sled.-e samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br />• (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) etbene; (d) 2-hexanone; (e) dichloromethane; (1) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than —5 vol. % <br /> sediment; (i) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br />