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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hap//www.mccamnbell.com E-mail mam@mccampbell corn <br /> Date Sampled 12/23/98 <br /> Advanced GeoEnvironmental Client Project ID Cherokee Truck Stop <br /> Date Received 12/24/98 <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact Kevin Mckibben Date Extracted 01/03/99 <br /> Client P O Date Analyzed 01/03/99 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 00877 <br /> Client ID UST-3112-23-98 <br /> Matnx W <br /> Compound Concentration* Compound Concentration" <br /> Acetone MND<3 Ethylbenzene 13 <br /> Benzene 18 Hexachlorobutadiene NO <br /> Bromobenzene NO lodomethane NO <br /> Bromochloromethane ND Isopropylbenzene NO <br /> Bromodichloromethane NO p-Isopropyl toluene NO <br /> Bromoform ND Methyl butyl ketone NO <br /> Bromomethane NO Methylene Chloride"' NO <br /> n-Butyl benzene NO Methyl ethyl ketone ND <br /> i} sec-Butyl benzene NO Methyl isobutyl ketone Is ND <br />!■� tert-Butyl benzene NO Methyl Cert-Butyl Ether(MTBE) <br /> Carbon Disulfide NO Napthalene NO <br /> Carbon Tetrachloride NO n-Propyl benzene NO <br /> Chlorobenzene NO Styrene M NO <br /> Chloroethane NO 1,1,1,2-Tetrachloroethane NO <br /> 2-Chloroethyl Vinyl Ether` NO 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> Chloromethane NO Toluene 94 <br /> 2-Chlorotoluene NO 1,2,3-Tnchloroberizene NO <br /> 4-Chlorotolucne NO 1,2,4-Tnchlorobenzene ND <br /> Dibromochloromethane NO 1,1,1-Tnchloroethane NO <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Tnchloroethane NO <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Tnchloroflueromethane ND j <br /> 1,3-Dichlorobenzene ND 1,2,3-Tnchloropropane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Tnmethylbenzene NO <br /> Dichlorodifluoromethane ND 1,3,5-Tnmcthylbenzene NO <br /> l,]-Dichloroethane ND Vinyl Acetate"I NO <br /> 1,2-Dichloroethane ND Vmyl Chloride " NO <br /> 1,1-Dichloroethene NO Xylenes,total 69 <br /> cis-1,2-Dichloroethene NO <br /> trans-l,2-Dichloroethene NO <br /> 1,2-Dichloropropane ND <br /> 1,3-Dichl01`opropane ND <br /> 2,2-Dichloropropane ND Comments <br /> 1,1-Dichloropropene NO Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND Dibromofluoromethane 101 <br /> trans-1,3-Dichloropropene ND Toluene-d8 90 <br /> Ethylene dibromide NO 4-Bromofluorobenzene 87 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 0 ug/L, vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe NO means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment,O)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,(1)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />