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4 <br /> 110 2nd Avenue South,#D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> ++ Eit$P l/www mccampbell cam E-mail mamQmccampbellconi <br /> Advanced GeoEnvtronmental, Inc Client Protect ID Cherokee Trucking Date Sampled 08/29/02 <br /> i837 Shaw Road Date Received 08/30/02 <br /> Stockton, CA 95235 CIient Contact Paul Dotson Date Extracted 08/30/02-09/06/02 <br /> Client P O Date Analyzed 08/30/02-09/06/02 <br /> Volatiles Organics+Oxygenates by P&T and GC/1VIS(Basic Target List)* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0208519 <br /> Lab ID 0208519-002C <br /> Client ID UST3/082902 <br /> Matrix Water <br /> RepWing <br /> Compound Concentration* DF Li,nit Compound Concentration* DF Urnitg <br /> Acetone ND 1 0 50 tert-Amyl methyl ether(TAME) ND 10 0 5 <br /> Benzene ND 10 0 5 Bromobenzene ND 10 0 5 <br /> Bromochloromethane ND 10 0 5 Bromodichloromethane ND 1 0 0 5 <br /> Bromofonn ND 1 0 0 5 Bromomethane ND 1 0 0 5 <br /> 2-Butanone(MEK) ND 1 0 1 0 t-Butyl alcohol(TBA) ND 10 5 0 <br /> n-Butyl benzene ND 10 0 5 sec-Butyl benzene ND 10 0 5 <br /> tert-Butyl benzene ND 10 0 5 Carbon Disulfide ND 1 0 0 5 <br /> Carbon Tetrachloride ND 1 0 0 5 Chlorobenzene ND 1 0 0 5 <br /> Chloroethane ND 10 0 5 2-Chlorcethyl Vinyl Ether ND 10 1 0 <br /> Chloroform ND 10 0 5 Chloromethane ND 1 0 0 5 <br /> 2-Chlorotoluene ND 10 0 5 4-Chlorotoluene ND 1 0 0 5 <br /> Dibromochloromethane ND 1 0 0 5 1,2-Dibromo-3-chloropropane ND 10 1 0 <br /> 1,2-Dibromoethane(EDB) ND 1 0 0 5 Dibromomethane ND 10 0 5 <br /> 1,2-Dichlorobenzene ND 1 0 0 5 1,3-Dichlorobenzene ND 10 0 5 <br /> 1,4-Dichlorobenzene ND 1 0 0 5 Dichlorodifluoromethane ND 1 0 0 5 <br /> • 1,1-Dichloroethane ND 10 05 ],2-Dtchlomethane(1,2-DCA) ND 10 05 <br /> 1,1-Dichloroethene ND 1 0 0 5 1 cis-1,2-1]tchloroethene ND 10 0 5 <br /> trans-l,2-Dichloroethene ND 1 0 0 5 1,2-D,chloropropane ND 10 0 5 <br /> 1,3-Dichloropropanc ND 1 0 0 5 2,2-Dichloropropane ND 10 0 5 <br /> 1,1-Dichlotopropene ND 1 0 6-5— cis-1,3-Dichloropropene ND 1 0 0 5 <br /> trans-l,3-Dichloropropenc ND 1 0 05 Dusopropyl ether(DIPC) ND 10 0 5 <br /> Ethylbenzene ND 1 0 0 5 Fthyl tert-butyl ether(ETRE) ND 1-0 0 5 <br /> Hexachlorobutadiene ND 1 0 5 0 2-Hexanone ND 1 0 0 5 <br /> Iodomethane(Methyl iodide) ND 1 0 0 5 Isopropylbenzene ND 10 05 <br /> 4-Isopropyl toluene ND 1 0 05 Methyl-t-butyl ether(MTBE) ND 10 05 <br /> Methylene chloride ND 1 0 0 5 4-Methyl-2-pentanone(MI13K) ND to 05 <br /> Naphthalene ND 1 0 5 0 n-Propyl benzene ND 10 05 <br /> Styrene ND 1 0 0 5 1,1,1,2-Tetrachloroethane ND 10 05 <br /> 1,1,2,2-Tetrachloroethane ND 1 0 0 5 Tetrachloroethene ND 10 05 <br /> Toluene ND 1 0 05 1,2,3-Tnchlorobenzene ND 10 05 <br /> 1,2,4-Tnchlorobenzene ND 1 0 0 5 1,1,1-Tnchloroethane ND 10 05 <br /> 1,1,2-Trichloroethane ND 1 0 05 Tricbloroethene ND 10 05 <br /> Tnchlorofluoromethane ND 1 0 05 1,2,3-Tnchloropropane ND l 0 05 <br /> 1,2,4-Trimethylbenzene ND 10 05 1,3,5-Tnmethylbenzene ND 1 0 05 <br /> Vinyl Acetate ND 10 5 0 Vinyl Chloride ND 10 05 <br /> Xylenes ND 1 0 0 5 <br /> Surrogate Recoveries(%) <br /> %SSI 105 %SS2 105 <br /> %SS3 972 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported to ug/L,soil/sludge/solid samples in ug/kg, wipe samples in ug/wipe, <br /> product/oil/non-aqueous liquid samples in mglL <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> • h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />