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110 2nd Avenue South ND7,Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1626 Fax 925-798-1622 <br /> zo I Website www mccanipbell corn E mail inainQmccampbell corn <br /> Advanced GeoEnvironmental, Inc Client Project ID Cherokee Truck Stop Date Sampled 03/12/04 <br /> Date Received 03/16/04 <br /> 837 Shaw Road <br /> Client Contact Paul Dotson Date Extracted 03116/04-03/17/04 <br /> Stockton, CA 95215 Client P O Date Analyzed 03/16/04-03/17/04 <br /> Volatiles Organics by P&T and GC/MS(Basic Target List)* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0403245 <br /> Lab ID 0403245-001 B <br /> Client ID UST 2 <br /> Matrix Water <br /> Compound I Concentration* DF <br /> Repont Compound Concentration* DF x Lmut <br /> Acetone ND 10 50 Acrolem(Pro enal) ND 10 so <br /> Acrylonitrile ND 10 20 tert-Amyl methyl ether(TAME) ND 10 05 <br /> Benzene ND 10 0 5 Bromobenzene ND 1 0 0 5 <br /> Bromochloromethane ND 10 0 5 Bromodichloromethane ND 1 0 05 <br /> Bromoform ND 1 0 0 5 Bromomethane ND 1 0 05 <br /> 2-Butanone(MEK) ND 1 0 1 0 t-Bu I alcohol(TBA) ND 1 0 50 <br /> n-13u I benzene ND 1 0 05 sec-Butyl benzene ND 1 0 05 <br /> tert-But l benzene ND 1 0 05 Carbon Disulfide ND 1 0 0 5 <br /> Carbon Tetrachloride ND 10 0 5 Chlorobenzene ND 1 0 05 <br /> Chloroethane ND 10 05 2-Chloroeth l Vinyl Ether ND 1 0 1 0 <br /> Chloroform ND 10 05 Chloromethane ND 1 0 05 <br /> 2-Chlorotoluene ND 10 05 4-Chlorotoluene ND 1 0 05 <br /> _Dlbromochloromethane ND 10 05 1,2-Dtbromo-3-chloro ro ane ND 1 0 0 5 <br /> 1,2-Dibromoethane(EDB) ND 10 05 Dtbromomethane ND 1 0 05 <br /> 1,2-Dichlorobenzene ND 1 0 0 5 1,3-Dichlorobenzene ND 1 0 05 <br /> 1,4-Dtchlorobenzene ND 1 0 0 5 Dichiorodifluoromethane ND 1 0 05 <br /> 1,1-Dichloroethane ND l 0 05 1,2-Dichloroethane(1,2-DCA) ND 1 0 05 <br /> 1,1-Dichloroethene ND 1 D 0 5 cis-1,2-Dichloroethene ND 1 0 05 <br /> trans-1 2-Dichloroethene ND l 0 0 5 1,2-Dichlororoane ND 1 0 0 5 <br /> 1,3-Dichlororopane ND 1 0 0 5 2,2-Dichlororo ane ND 10 0 5 <br /> IJ-Dichlororo ene ND 1 0 0 5 cis-1,3-Dichloro ra ene ND 1 0 05 <br /> trans-l,3-Dichlororopene ND 1 0 0 5 Diiso ro l ether(DIPS) ND 1 0 05 <br /> Eth ]benzene ND 1 0 05 Ethyl tert-butyl ether ETRE) ND 1 0 05 <br /> Hexachlorobutadiene ND 1 0 0 5 Hexachloroethane ND 1 0 1 0 5 <br /> 2-Hexanone ND 10 0 5 Isopropylberizene ND 1 0 0 5 <br /> 4-1so rol toluene ND 10 0 5 Meth i-t-but 1 ether MTBE ND 1 0 0 5 <br /> .Methylene chloride ND 10 0 5 4-Methyl-2- entanone MIBK ND 1 0 0 5 <br /> Naphthalene ND 1 0 0 5 Nitrobenzene ND 1 0 10 <br /> n-Propyl benzene ND 1 0 0 5 Styrene ND l 0 05 <br /> 1,1,1,2-Tetrachloroethane ND 10 05 1,1,2,2-Tetrachloroethane ND l 0 0 5 <br /> Tetrachloroethene ND 1 0 05 Toluene 066 l 0 0 5 <br /> 1,2,3-Tnchlorobenzene ND 10 05 1,2,4-Trichlorobenzene ND l 0 0 5 <br /> 1,1,1-Trichloroethane ND 10 05 1,1,2-Trichloroethane ND l 0 05 <br /> Trichloroethene ND to 05 Trichlorofluoromethane ND 10 05 <br /> 1,2,3-Tnchloro ro ane ND 10 05 1,1,2-Trichloro-I 2,2-trifltlUrnethane ND 10 t0 <br /> 12,4-Trimethylbenzene ND [D 05 1,3,5-Tnmeth (benzene ND 10 05 <br /> Vm i Chloride ND l 0 0 enes 052 10 1 05 <br /> Surrogate Recoveries(%) <br /> %SSI 105 %SS2 986 <br /> %SS3 100 <br /> Comments <br /> *water and vapor samples and ail TCLP&SPLP extracts are reported inµg/L,soil/sludgelsolid samples in lig/kg, wipe samples inµg/wipe <br /> product/oil/non-aqueous liquid samples in mg1L. <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 '-'V Angela Rydehus, Lab Manager <br />