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McCampbell Analytical, Inc. tl02lephone 25-799-16 Pacheco,92 - 98-1622SfiO
<br /> Telephone 925-798-1620 Fax 925-798-1622
<br /> Website www trrcampbell com E-mail mam®mccampbell com
<br /> Advanced GeoEnvironmental, Inc Client Project ID Cherokee Truck Stop Date Sampled 03/12/04
<br /> . 837 Shaw Road Date Received 03/16/04
<br /> Client Contact Paul Dotson Date Extracted 03/16/04-03/17/04
<br /> Stockton,CA 95215 Client P O Date Analyzed 03/16/04-03/17/04
<br /> Volatiles Organics by P&T and GC/MS(Basic Target List)*
<br /> Fxtracnon Method SW503013 Analytical Method SW8260B Work Order 0403245
<br /> Lab ID 0403245-00313
<br /> Client ID UST 4
<br /> Matnx Water
<br /> Repoing
<br /> Compound Concentration* DF Lumt`gpo
<br /> L
<br /> Compound Concentration * DF R°inin
<br /> ntnt
<br /> Acetone ND 1 0 50 Acrolein(Propenal) ND 1 0 so
<br /> Acrylonitrile ND 1 0 20 Cert-Amyl methyl ether AME ND 10 05
<br /> Benzene ND to 05 Bromobenzene ND 10 05
<br /> Bromochloromethane ND 10 05 Bromodichloromethane ND 10 05
<br /> Bromoform ND 10 0 5 Bromomethane ND 10 05
<br /> 2-Butanone MEK ND to 10 t-Butyl alcohol(TBA) ND 10 50
<br /> n-Bu l benzene ND 10 05 sec-Bu!yl benzene ND to 05
<br /> tert-Butyl benzene ND 1 0 05 Carbon Disulfide ND 10 05
<br /> Carbon Tetrachloride ND 10 05 Chlorobenzene ND 1 0 05
<br /> Chloroethane ND 1 0 05 2-Chloroeth1 Vinyl Ether ND 10 1 0
<br /> Chloroform ND 1 0 05 Chloromethane ND 1 0 05
<br /> 2-Chlorotoluenc ND 10 05 4-Chlorotoluene ND 1 0 05
<br /> Dibromochloromethane ND 10 05 1 2-Dibromo-3-chloro ro ane ND 1 0 05
<br /> 1,2-Dibromoethane(ED ND 10 05 Dibromomethane ND 1 0 05
<br /> 1,2-Dichlorobenzene ND 10 0 5 1,3-Dichlorobenzene ND 1 0 0 5
<br /> 1 4-Dichlorobenzene T ND 1 0 05 Dichlorodifluaromethane ND 10 05
<br /> . 1 I-Dtchloroethane ND 10 05 1,2-Dlchloroethane(1,2-DCA) ND i lo 05
<br /> 1,1-Dichloroethene ND to 05 cis-1,2-DichloroetheneND 1 0 0 5
<br /> trans-l,2-Dichloroethene ND 10 05 1,2-Dichlororo ane ND ' 10 05
<br /> 1,3-Dichlororoane ND 10 0 5 2,2-Dichloro roane ND l 0 05
<br /> I,1-Dichloropro ene ND 1 0 05 1 cis-1,3-Dichlororo ene ND 1 0 05
<br /> trans-l,3-Dichlororoene ND 1 0 05 Diiso rol ether(DIPE) ND 10 05
<br /> Eth lbenzene ND 1 0 05 Ethyl tert-bu 1 ether ETBE ND 1 0 05
<br /> Hexachlorobutadiene ND 1 0 05 Hexachloroethane ND to 05
<br /> 2-Hexanone ND 1 0 0 5 Isopropylbenzene ND to 05-
<br /> 4-isopropyl
<br /> 54-]so ro l toluene ND 10 0 5 Meth l-t-but l ether MTBE ND 10 0 5
<br /> Meth lene chloride 0 84 10 0 5 4-Meth 1-2- entanone(MIRK) ND 10 0 5
<br /> Naphthalene ND l 0 0 5 Nitrobenzene ND 10 I0
<br /> n-Propyl benzene ND 1 0 05 Styrene ND 1 0 0 5
<br /> 1,1,1,2-Tetrachloroethane ND 1 0 0 5 1,1,2,2-Tetrachloroethane ND 1 0 0 5
<br /> Tetrachloroethene ND l 0 0 5 Toluene ND 1 0 0 5
<br /> 1,2,3-Tnchlorobenzene ND 1 0 0 5 1,2,4-Trichlorobenzene ND 1 0 0 5
<br /> 1,1,1-Trichloroethane ND 10 0 5 1,1,2-Trichloroethane ND 1 0 05
<br /> Trichloroethene ND 1 0 0 5 Tnchlorotluoromethane ND 10 05
<br /> 1,2,3-Trichloro ro ane ND 1 0 0 5 1,1,2-Tnchloro-1,2,2-trifluoroethane ND 10 10
<br /> 1,2,4-Trimeth (benzene ND 10 0 5 1,3,5-Tnmeth (benzene ND 10 0 5
<br /> Vinyl Chloride ND 1 10 05 Xylenes ND i 10 0 5
<br /> Surrogate Recoveries(%)
<br /> %SS1 77-7 106 7%SS2 969
<br /> %SS3 101
<br /> Comments
<br /> «water and vapor samples and all TCLP&SPLP extracts are reported in ltg/L,soilisludge/solid samples inµg/kg, wipe samples to jig/wipe,
<br /> product/oil/non-aqueous liquid samples in mg/L
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> #surrogate diluted out of range or surrogate coelutes with another peak
<br /> h)lighter than water immiscible sheen/product is present i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high
<br /> organic content
<br /> DHS Certification No 1644 Angela Rydeltus, Lab Manager
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