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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925 798 1620 Fax 925-798 1522 <br /> ht Jlwww nicca bell com 1:mad mam cca hell com <br /> Advanced GeoEnvironmental,Inc Client Project ID Cherokee Truck Stop Date Sampled 09/25/03 <br /> 837 Shaw Road Date Received 09/26/03 <br />' Client Contact Paul Dotson Date Extracted 09/30/03-10101103 <br /> Stockton,CA 95215 <br /> rCl-ientP O Date Analyzed 09/30/03-10101/03 <br /> Volatiles Organics+Oxygenates by P&T and GC/MS(Basic Target List)* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0309482 <br /> Lab 1D 0309482-007C <br /> Client ID DWI <br /> Matrix Water <br /> Compound Concentration* DF x =8 Compound Concentration " DF <br /> Acetone ND 10 50 tent-Amyl methyl ether TAME ND 1 0 0 5 <br /> Benzene ND 10 0 5 Bromobenzene ND 1 0 0 5 <br /> Bromochloromethane ND 10 0 5 Bromodichloromethane ND 10 0 5 <br /> 13romoform ND 10 0 5 Bromomethane ND 1 0 0 5 <br /> I 2-Butanone EK) ND to 10 t-Butyl alcohol TBA ND 1 0 5 0 <br /> n-Butyl benzene ND to 05 sec-Butyl benzene ND 1 0 05 <br /> tert-Butyl benzene ND to 0 5 Carbon Disulfide ND 10 0 5 <br /> Carbon Tetrachloride ND 10 D 5 Chlorobenzene ND 1 0 0 5 <br />' Chloroethane ND 1 0 D 2-Chloro ND <br /> 10 05 <br /> Chloroform ND 10 0 5 Chloromethane ND 1 0 05 <br /> 2-Chlorotoluene ND l 0 05 4-Chlorotoluene ND 1 0 0 5 <br /> Dibromochloromethane ND l 0 05 1,2-Dibrotno-3-chlororo ane ND 1 0 0 5 <br /> 1 2-Dibromoethane EDB ND l 0 0 5 Dibromomethane ND 1 0 05 <br /> 1,2-Dichlorobenzene ND 1 0 05 1,3-Dichlorobenzene ND 1 0 05 <br /> 1,4-Dichlorobenzene ND 1 0 05 Dichlorodifluoromethane ND 1 0 05 <br />' <br /> 1,1-Dwhloroethane ND l0 05 1,2-Dichloroethane 1,2-DCA ND 10 05 <br /> 1,1-Dichloroethene ND to 05 cis-1,2-Dichloroethcne ND to 05 <br /> trans-1,2-Dichloroethene ND 1 0 0 5 1 2-Dichloro ro ane ND 1 0 o5 <br /> 1,3-Dichloro ra ane ND 1 0 0 5 2 2-Dichloro ro ane ND 1 0 0 5 <br />' 1,l-Dichlororo ene ND 1 0 0 5 cis-1 3-Dichloro ro ene ND I 0 05 <br /> trans-l,3-Dichloro ropene ND 1 0 05 Dnso ro 1 ether DIPS ND to 05 <br /> Eth (benzene ND 1 0 0 5 Ethyl tert-but l ether(ETBE) ND to o 5 <br /> Hexachiorobutadiene ND 1 0 05 2-Hexanone ND 1 0 05 <br />' Iodomethane(Methyl iodide ND 1 0 50 Iso ro ylbenzene ND 1 0 0:5 <br /> 4-lsopt-opyii toluene i ND 1 0 0 5 Meth 1-t-but l ether MTBE ND 1 0 0 5 <br /> Methylene chloride ND 1 0 0 5 4-Meth 1-2- entanone(MIBK) ND 1 0 0 5 <br /> Naphthalene ND 1 0 0 5 n-Pro yl benzene ND 1 0 1 0 5 <br /> I <br /> Styrene ND 10 0 5 1,1,1,2-Tetrachloroethane ND l 0 o5 <br /> 1,1,2 2-Tetrachloroethane ND 10 05 Tetrachloroethene ND 1 0 05 <br /> Toluene ND 1 0 05 1,2,3-Tnehlorobenzene ND 1 0 05 <br /> 1,2,4-Tnehlorobenzene ND 1 0 05 1,1,1-Tnchloroethane ND 10 05 <br />' 1,1,2-Trichloroethane ND 1 0 05 Trichloroethene ND 1 0 05 <br /> Trichlorofluoromethane ND l 0 05 1,2,3-Tnchlororo ane ND 1 0 05 <br /> 1 2,4-Trmeth !benzene ND 10 05 1,3 5-Trimeth ]benzene ND 1 o——0 5 <br /> Vinyl Acetate ND 10 50 Vinyl Chloride ND _—to 1 05 <br />' <br /> Xylenes ND 10 05 <br /> Surrogate Recoveries <br /> %SSI 113 %SS2 105 <br />' °/uSS3 99 2 <br /> Comments <br /> 'water and vapor samples and all TCLP&SPLP extracts are reported inµglL,soillsludgelsolid samples inµgfkg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mglL <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> 0 #surrogate diluted out of range or surrogate coelutes with another peak <br />' h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than–2 vol %sediment,3)sample diluted due to high <br /> or atilt content <br />' DHS Certification No 1644 Angela Rydelrus, Lab Manager <br />