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SEQUOIA ANALYTICAL <br /> 680 Chesapeake Drive • Redwood City, CA 94063 <br /> (415) 364-9600 FAX (415) 364-9233 <br /> .P:S{n:'S-0t Yn;n:L.::ti?:?vi}}Yi^}xi nQ:}':{:mv,{{.}:S•}:±:::{:}i^ <br /> . . <br /> ' :N..±�f{{{.:M:±•: <br /> .... .......... ...... v:vw::.w:n.::.•:•{.}}:ttM.M::vr::Sd}:{{:v.±{•.vfh.d}. .{•'F.if..::?{'3'.2•:n ...:.h.v4n .. <br /> ........................ x:......x.........x....v,..}}..........{...t......n:...........:................:..'.K.v:• .......'.tom--�............ti::::.:.::::::....:. ...}:"}Y:" ..... i...... ..n. <br /> ...................................................:::..r.......v:::::;•:::::::.v::::::.....:........:::. :-.v:::::::::........;..:::.::.Y;\}l.:%Ivv,•:}r:::r:F}}�.i}.:ft�•:JGT''4YN:?}:r..:r}::::::::::..:}Y.•n.i/..1.h�i.:i}:•}:{•i:•:::is::iv}:h:}mL:S'lM}:n1Sn'•}:v':}'::'•}::: <br /> �RESNA:...................:..'.r.............:.»rr.............:...::<±Clerit�Project�ID • 780013.01, Newark Sierra <br /> €2134 Rheem Drive, Suite B Matroc: Solid ' <br /> ::::Pleasanton, CA 94588 ' <br /> DC Sample Group: 3K66101-06 <br /> Attention: John Lamb Reported. Nov 23, 1993 <br /> ............................w:,t•:.vv•:w-v x•,:vnw:.. -mm�'.y^Y.4:}}vp!h%i^PY.•}M.\`Y.?{M^%:"4Y.^:K:'}:?p:.Y.•:.yi}x ;M:, F..::'i:?ij'i'r'r}:::C:`:isisn:}.y}�C.,v{MifM?}:;•:.::jii:?::vi:}:i' <br /> ............................. .....rr..........n•• .n....................• ....-:::::..........................;..;;}..{3 v::nv:.v.•.:.:.....v:.4..v. ...i.. rx:. ...:..... <br /> ....................................... .................................:.w:::•.v.v:.v:•w:}:::::::n...r... 3:. v..:. .n. .n........ .v...............vtOt{tM4.Kv.::.v.•.:{^:{S•.v:r:x6}:::±riti4:•JiS•}:4}:•}:v{{.}}ri•}:4}: <br /> ..............................................{.}}}:q}:•}:4:?-}}}}:•}ii}:^:S4?ii5�:::•::.w.:v.v:•.vvn•.x::vxv::1::{r.:\ti4:fit:..}h.pvnJL:{...\:...........{v.•.7SbAYIi.:•. ••:i�f.SS.r.,r:.v::::::: <br /> QUALITY CONTROL DATA REPORT <br /> ANALYTE Diesel <br /> M.£t.+od: EPAso.3 Mod. <br /> Analyst: D.Tran <br /> MS/MSD <br /> Batch#: 3K66103 <br /> Date Prepared: 11/15/93 <br /> Date Analyzed: 11/17/93 <br /> Instrument I.D.#: GCHP-4A <br /> Conc. Spiked: 15 mg/kg <br /> Matrix Spike <br /> % Recovery: 84 <br /> Matrix Spike <br /> Duplicate% <br /> Recovery: 86 <br /> Relative% <br /> Difference: 2.4 <br /> ..n..Stiiii$:Y........r..x....................n...:.n..:...:..:.r..:..r.n.n......v..................... <br /> LCS Batch#: eLK111593 <br /> Date Prepared: 11/15/93 <br /> Date Analyzed: 11/17/93 <br /> Instrument I.D.#: GCHP-4A <br /> LCS % <br /> Recovery: 100 <br /> %Recovery <br /> Control Limits: 38-122 <br /> _ Please Note: <br /> - The LCS is a control sample of known,interferent free matrix that is analyzed using the same reagents, <br /> SEQUOIA ANALYTICAL preparation,and analytical methods employed for the samples. The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure. If <br /> the recovery of analytes from the matrix spike does not fall within speed control limits due to matrix <br /> `{C�J✓tom— interference,the LCS recovery is to be used to validate the batch. <br /> Vickie Tague <br /> Project Manager 3K66101.RES <4> <br />