110 2nd Avenue South,#D7,Pacheco,CA 94553-5560
<br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622
<br /> httn llwww mccamnbell corn E-mail main@mccampbell com
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<br /> Advanced GeoEnvironmental Client Project ID DSS- Stockton Date Sampled 07/23/99
<br /> 4005 North Wilson Way Date Received 07/27/99
<br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 07/27/99
<br /> Client P O Date Analyzed 07/30/99
<br /> EPA method 8260 Volatile Organics By GCIMS
<br /> Lab ID 16070
<br /> Client JD P2-5
<br /> Matrix S
<br /> Compound Concentration* ComRound Concentration*
<br /> Acetone 16i ND trans-l,3-Dichloropropene ND
<br /> Benzene ND Ethylene dibromide ND
<br /> Bromobenzene ND Ethylbenzene ND
<br /> Bromochloromethane ND Hexachlorobutadiene ND
<br /> Bromodichloromethane ND Iodomethane ND
<br /> Bromoform ND Isopropylbenzene ND
<br /> Bromomethane ND -Iso ropyl toluene ND
<br /> n-Butyl benzene ND Methyl butyl ketone 1°' ND
<br /> sec-Butyl benzene ND Methylene Chloride" ND<15
<br /> tert-Butyl benzene ND Methyl ethyl ketone" ND
<br /> Carbon Disulfide ND Methyl isobutyl ketone asi ND
<br /> Carbon Tetrachloride ND Methyl tert-B utyl Ether(MTBE) —.
<br /> Chlorobenzene ND Naphthalene ND
<br /> Chloroethane ND n-Propyl benzene ND
<br /> 2-Chloroeth I Vinyl Ether") ND Styrene"i ND
<br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND
<br /> Chloromethane ND 112,2-Tetrachloroethane ND
<br /> 2-Chlorotoluene ND Tetrachloroethene ND<10
<br /> 4-Chlorotoluene ND Toluene"' ND
<br /> Dibromochloromethane ND 12,3-Trichlorobenzene ND
<br /> 1,2-Dibromo-3-chloro ro ane ND 1,2,4-Trichlorobenzene ND
<br /> Dibromomethane ND 1,1,1-Trichloroethane ND
<br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND
<br /> 1,3-Dichlorobenzene ND Trichloroethene ND
<br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane ND
<br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND
<br /> 1,J-Dichloroethane ND 1,2,4-Tri methyl benzene ND
<br /> 1,2-Dichloroethane ND 1,3,5-Trimethylbenzene ND
<br /> 1,1-Dichloroethene ND Vinyl Acetate""i ND
<br /> cis-1,2-Dichloroethane ND Vinyl Chloride"°i ND
<br /> trans-I,2-Dichloroethene ND X Ienes,total 1pr ND
<br /> 1,2-Dichloro ro ane ND Comments
<br /> 1 3-Dichloro ro anc ND Surrogate Recoveries
<br /> 2,2-Dichloro ropane ND Dibromofluoromethane 102
<br /> I,1-Dichloropropene ND Toluenc:A8 105
<br /> cis-1,3-Dichloro ro ane ND 4-Bromofluorobenzene 102
<br /> 'water and vapor samples are reposed in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L
<br /> Reporting limits unless otherwise stated water samples I ug/L. vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> • (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2-
<br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol %
<br /> sediment 0) sample diluted due to high organic content (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester, (n)
<br /> chloroethene o methylbenzenes
<br /> DHS Certification No 1644 Edward Hamilton, Lab Director
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