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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> httn llwww mccamnbell corn E-mail main@mccampbell com <br /> s <br /> Advanced GeoEnvironmental Client Project ID DSS- Stockton Date Sampled 07/23/99 <br /> 4005 North Wilson Way Date Received 07/27/99 <br /> Stockton, CA 95205 Client Contact Kevin McKibben Date Extracted 07/27/99 <br /> Client P O Date Analyzed 07/30/99 <br /> EPA method 8260 Volatile Organics By GCIMS <br /> Lab ID 16070 <br /> Client JD P2-5 <br /> Matrix S <br /> Compound Concentration* ComRound Concentration* <br /> Acetone 16i ND trans-l,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND Iodomethane ND <br /> Bromoform ND Isopropylbenzene ND <br /> Bromomethane ND -Iso ropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone 1°' ND <br /> sec-Butyl benzene ND Methylene Chloride" ND<15 <br /> tert-Butyl benzene ND Methyl ethyl ketone" ND <br /> Carbon Disulfide ND Methyl isobutyl ketone asi ND <br /> Carbon Tetrachloride ND Methyl tert-B utyl Ether(MTBE) —. <br /> Chlorobenzene ND Naphthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroeth I Vinyl Ether") ND Styrene"i ND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane ND <br /> Chloromethane ND 112,2-Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND<10 <br /> 4-Chlorotoluene ND Toluene"' ND <br /> Dibromochloromethane ND 12,3-Trichlorobenzene ND <br /> 1,2-Dibromo-3-chloro ro ane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1,1-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2,3-Trichloropropane ND <br /> 1,J-Dichloroethane ND 1,2,4-Tri methyl benzene ND <br /> 1,2-Dichloroethane ND 1,3,5-Trimethylbenzene ND <br /> 1,1-Dichloroethene ND Vinyl Acetate""i ND <br /> cis-1,2-Dichloroethane ND Vinyl Chloride"°i ND <br /> trans-I,2-Dichloroethene ND X Ienes,total 1pr ND <br /> 1,2-Dichloro ro ane ND Comments <br /> 1 3-Dichloro ro anc ND Surrogate Recoveries <br /> 2,2-Dichloro ropane ND Dibromofluoromethane 102 <br /> I,1-Dichloropropene ND Toluenc:A8 105 <br /> cis-1,3-Dichloro ro ane ND 4-Bromofluorobenzene 102 <br /> 'water and vapor samples are reposed in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples I ug/L. vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> • (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment 0) sample diluted due to high organic content (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethene o methylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />