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110 2nd Avenue South #137 Pacheco CA 94553-5560 <br /> �McCa�mpbe�IlAna�lyftcal Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> 740 http//www mccainpbell corn E-mail mam@mccampbell corn <br /> Advanced GeoEnviromnental,Inc Client Project ID West Clay Prop Date Sampled 05/28/02 <br /> 837 Shaw Road Date Received 05/29/02 <br />' Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 05/31/02-06/04/02 <br /> [C=hent Date Analyzed 05/31/02-06/04/02 <br />' Oxygenated Volatile Organics by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0205399 <br />' Lab ID 0205399-013C 0205399-014C 0205399-015C 0205399-016C <br /> Client ID MW11A/05-28- MW1 IB/05-28- MW12A/05-28- MW12B/05-28- Reporting Limit for <br />' <br /> Matrix WW W W OF—1 <br /> I <br /> DF 1 1 1 2 <br /> S W <br /> I <br />' Compound Concentration ug/kg pg/L <br /> Dusopropyl ether(DIPS) ND NO NO ND<1 NA 05 <br />' Ethyl tert-butyl ether(ETBE) NO NO ND ND<1 NA 05 <br />' Methyl-t-butyl ether(MTBE) ND 39 NO 37 NA 05 <br /> tert-Amyl methyl ether(TAME) NO NO NO ND<1 NA 05 <br /> t • t-Butyl alcohol(TBA) ND 83 ND ND<10 NA 5 <br /> Methanol ND<1000 ND<600 ND<600 ND<1000 NA 500 <br />' Ethanol NO NO ND ND<100 NA 50 <br />' 1,2-DEbrornoethane(EDB) NO ND NO ND<1 NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND 20 NO 17 NA 05 <br />' Surrogate Recoveries (%) <br /> %SS 108 107 109 108 <br />' Comments <br /> "water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L — <br />' ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water imnuscible sheen/product is present,(t)liquid sample that contains greater than—2 vol %sediment 0)sample diluted due to <br /> ihigh organic content <br /> i <br /> i <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br /> i <br />