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' 110 2nd Avenue South,#D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br />' httpJ/www mccanipbell com E mail maut@rnccanTbcJl com <br /> Advanced GeoEnvironmental, Inc Client Project ID West Clay Date Sampled 12/26/02 <br />' 837 Shaw Road Date Received 12/27/02 <br /> Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 12/27/02 <br />' Client P O Date Analyzed 12/27/02-01/03/03 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Amlytieal Method SW8260B Work Order 0212433 <br />' Lab ID 02I2433-00113 0212433-002B 0212433-003B 0212433-0048 <br /> Client ID MW-i MW-2 MW-3 MW-4 Reporting Limit for <br /> DF=1 <br />' Matrix W_ W T_— W- —W <br /> DF 1 2 1 1 1 S W <br /> i <br /> Compound Concentration gg/Kg pg/L <br />' tert-Amyl methyl ether(TAME) ND ND<l ND ND NA 05 <br /> Benzene ND 35 ND ND NA 05 <br /> I <br />' t-Butyl alcohol(TBA) ND ND<10 ND ND NA 5 0 <br /> 1,2-Dibmmoethane(EDB) ND ND<1 ND ND NA 0 5 <br /> 1,2-Dichloroethane(1,2-DCA) 0 79 20 ND ND NA 0 5 <br />' Dusopropyl ether(DIPE) ND ND<1 ND ND NA 0 5 <br /> Ethanol ND ND<100 ND ND NA 50 <br /> Ethylbenzene ND ND<1 ND ND NA 05 <br />'. Ethyl tert-butyl ether(ETBE) ND ND<1 ND ND NA 0 5 <br /> Methanol ND ND<1000 ND ND NA 500 <br /> Methyl-t-butyl ether(MTBE) ND ND<1 ND ND NA 0 5 <br />' Toluene ND 1 5 ND ND NA 0 5 <br /> Xylenes 0 69 160 ND ND NA 0 5 <br /> Surrogate Recoveries <br />' %SS 966 109 994 997 <br /> Comments <br /> water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/oillnon-aqueous liquid samples in mg/1- <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> i h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,,l)sample diluted due to high <br /> organic content <br /> i <br /> I <br /> I <br /> I <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />