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110 2nd Avenue South ND7 Pacheco CA 94553-5560 <br /> MCCampbell Analytical, Inc. Telephone 925 798 1620 Fax 925 798-1622 <br /> Website www mccarrilibell corn E-mail main@mccantpbell cont <br /> Advanced GeoEnvironmental,Inc Client Project ID West Clay-Ozone Date Sampled 04/01/05 <br /> BST Date Received 04/05/05 <br /> 837 Shaw Road <br /> Client Contact Bill Little Date Extracted 04/05/05 <br /> Stockton, CA 95215 Client P O Date Analyzed 04/14/05 <br /> Volatile Organics by P&T and GUMS(Basic Target List)* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0504049 <br /> Lab ID 0504049-008A <br /> Client 1D Soil Final <br /> Matrix Soil <br /> Reporting <br /> Compound Concentration* DF <br /> Repo g Compound Concentration * DF Lnn t <br /> Acetone ND<O 20 40 005 Acrolem(Pro enal) ND<O 20 40 005 <br /> Ac lonitnle ND<O 080 40 002 tert-Am l methyl ether AME ND<O 020 40 0 005 <br /> Benzene ND<O 020 4 0 0 005 Bromobenzene ND<O 020 4 0 0 005 <br /> Bromochloromethane ND<O 020 4 0 0 005 Bromodtchloromethane ND<O 020 40 0 005 <br /> Bromoform ND<O 020 4 0 0 005 1 Bromomethane ND<O 020 4 0 0 005 <br /> 2-Butanone(MEK) ND<O 080 4 0 002 t-But l alcohol A) ND<O 10 4 0 0 025 <br /> n-But 1 benzene 026 4 0 0 005 sec-But I benzene 0 065 4 0 0 005 <br /> tent-Butyl benzene ND<O 020 4 0 0 005 Carbon Disulfide ND<O 020 40 0 005 <br /> Carbon Tetrachloride ND<O 020 4 0 0 005 Chlorobenzene ND<O 020 4 0 0 005 <br /> Chloroethane ND<O 020 4 0 0 005 2-Chloroeth I Vinyl Ether ND<O 040 4 0 001 <br /> Chloroform ND<O 020 40 0 005 Chloromethane ND<O 020 4 0 0 005 <br /> 2-Chlorotoluene ND<O 020 40 0 005 4-Chlorotoluene ND<O 020 46 0 005 <br /> Dibromochloromethane ND<O 020 4 0 0 005 1,2-Dibromo-3-chloro ro ane ND<O 020 4 0 1 0 005 <br /> 1,2-Dibromoethane(EDB) ND<O 020 4 0 0 005 Dibromomethane ND<O 020 4 0 0.005 <br /> 1,2-Dichlorobenzene ND<O 020 4 0 0 005 1 3-Dichlorobenzene ND<O 020 4 0 0 005 <br /> 1 4-Dichlorobenzene ND<O 020 4 0 0 005 Dichlorodifluoromethane ND<O 020 4 0 0 005 <br /> 1 1-Dlchloroethane ND<O 020 4 0 0 005 1,2-Dichloroethane 1,2-DCA ND<O 020 4 0 .0005 <br /> • 1,1-Dichloroe1hene ND<O 020 4 0 0 005 cis-1,2-Dichloroetbene ND<O 020 4 0 0 005 <br /> trans-l,2-Dichloroethene ND<O 020 4 0 0 005 1 2-Dtchlororo dne ND<O 020 4 0 0 005 <br /> 1,3-Dichloro ro ane ND<O 020 4 0 0 005 2,2-Dtchloro ro ane ND<O 020 4 0 0 005 <br /> ],k-Dtchloro ro ene ND<O 020 4 0 0 005 cis-1,3-Dtchloro ro ene ND<O 020 4 0 0 005 <br /> trans-l,3-Dichloro ro ene ND<O 020 4 0 0 005 Duso ro 1 ether(DIPS) ND<O 020 4 0 0 005 <br /> Eth lbenzene 0 12 4 0 0 005 Ethyl tert-but 1 ether(ETBE) ND<O 020 4 0 0 005 <br /> Freon 113 ND<O 40 M40 <br /> 1 Hexachlorobutadiene ND<O 020 4 0 0 005 <br /> Hexachloroethane ND<O 020 0 05 2-Hexanone ND<O 020 4 0 0 005 <br /> Iso ro lbenzene 0 037 0'o 05 4-Isopropyl toluene ND<O 020 4 0 0 005 <br /> Meth l-t-but 1 ether MTBE ND<O 020 4 0 0 005 Methylene chloride ND<O 020 4 0 0 005 <br /> 4-Meth 1-2- entanone MIBK ND<O 020 4 0 0 005 Na hthalene 0 17 4 0 0 005 <br /> Nitrobenzene ND<O 40 4 0 0 1 n-PTopyl benzene 0 22 4 0 0 005 <br /> S ene ND<O 020 4 0 0 005 1,1,1,2-Tetrachloroethane ND<O 020 4 0 0 005 <br /> 1,1,2,2-Tetrachloroethane ND<O 020 4 0 0 005 Tetrachloroethene ND<O 020 4 0 0 005 <br /> Toluene ND<O 020 40 1 0 005 1,2,3-Trichlorobenzene ND<O 020 40 0 005 <br /> 1 2 4-Trichlorobenzene ND<O 0200 0 005 1,1,1-Trichloroethane ND<O 020 4 0 0 005 <br /> 1,1 2-Trichloroethane ND<O 020t�40 0005 Trichloroethene ND<O 020 4 0 0005 <br /> Trichlorofluoromethane ND<O 0204 0 0 005 1,2,3-Trichloro ro ane ND<O 020 4 0 0 005 <br /> 1,2,4-Trimethylbenzene 0 82 40 0 005 1,3,5-Trtmethyibenzene 0 045 4 0 0 005 <br /> Vinyl Chloride ND<O 020 1 4 0 0 005 Xylenes 0 35 4 0 1 0 005 <br /> Surrogate Recoveries(%) <br /> %SSI 92 %SS2 97 <br /> %SS3 114 <br /> Comments <br /> *water and vapor samples are reported in lig/L,soil/sludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP <br /> extracts are reported in mg/L,wipe samples in gg/wipe <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—1 vol %sediment,j)sample diluted due to high <br /> organic comcntlmatrix interference,k)reporting limit near,but not identical to our standard reporting limit due to variable Encore sample weight m) <br /> reporting limit raised due to insufficient sample amount,n results are reported on a dry weight basis, see attached narrative <br /> DHS Certification No 1644 44C— Angela Rydelius, Lab Manager <br />