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1 110 2nd Avenue South #D7 Mcheco CA 9453 5 60 McCampbell Analytical, Inc. Telephone 925 796-1620 Fax 925 795 1622 t t Web5lte www niceampbell coin E mall main a+nrLcampbell cam Advanced GeoEnvlronmental, Inc Client Ptoject ID West Clay- Ozone Date Sampled 04/05/05 BST Date Received 04/05/05 S37 Shaw /toad Client Contact Bill Little Date Extiacted 04/05/05 Stockton, CA 95215 Client P O Date Analyzed 04/13/05 Volatile Organics by P&T and (X/MS (Basic Target List)* F\lr1e11011 Methad SW�,0306 Analytical Method SW6260B Wort.Oo der 0.04049 Lab-1 D __-- - — _ -- _ _0504049_010A- Client ]D --- - _ _ Ozone_Degassed_Back Matrix Sol] Reponing1{ep°sting Compound Concentiatlon -I' DF Limit Compound Concentration * DF L,n,,, Attune ND<O 015 to-1 0 OS A_ciolem(Pi openal) - ND<O 01 s k 11 005 Acrylonitille _ND<O 0060_ 1_0—_— 0 02 tert Amyl methyl ether(TAME) - ND<O 0015 10 U QUA _ _ - Benzene __ _ __0_0052 i LO i_0 405_ BromoUenND<O 0015 10 0 005zene -� _ ,_ _ BI OtnOLM010111ethane _ _ ND<0 0015 _10_1 0005 Bromodlch_1_oromethane— ___ '_ ND<O 0015 10 0 005 4tamotolm _ ND<0 0015 10_ 1 0005 Bromomethane _ ND<O 0015 ]0 {}005 2 Butanone(MEK) _ 0 0_91 1QT__ 002 t Butyl alcoh_o1(TBA)— -_- N_D<0 0075 10 U 02� II-Butyl benzene ND<O 0015 10 00o5_ -sec-Butyl benzene- - ND<O 0015 10 0 00s tett-Butyl bcilzene ND<O 0015 W 10_ I 0005 _Carbon Disulfide_ ND<O 0015 10 0 005 ( uboii Tc11 tc11101ide ND<0 0015 10 0 005 Chloiobenzene ND<O 001� 10 000S C Nolooll 1ne ND<O 0015 10 0 005 _2-Chlornethyl Vinyl Ethel ND<O 0030 10 001 { 111010101/11 ND<O 0015 10 0 005 Chloromethane ND<O 0011, 10 0(M9 2 Chlorotolowne ND<O 0015 10 0005 4-C_hlo_rotoluene_ _ _ ND<0 0015 10 0 00'� Dibiomochlowmethane ND<O 0015 _ l0- 0 005 1_2-Dlbromo-3-chlolopropane ND<O 001 10 U 005 1 2 DiN onloethane(EDB) ND<0 0_015 10 0 005 Dibro_momethane_ _ - _ _ND_<0 0015 to 0 005 - 7- - 1 2 D1c111niobenzertc N1a<0 0015 r1_0 0 005 l,3-Dlch1olobenzene _ T -_ _ ND<0 0_015 10 0 005 D 1 4 iLliloicbenzene ND<O 0015_ _ _10 0 005 Dichlorodifluoromethane_ ND<O 0015 I(l 0 0O5 1 I Dlchlomethane ND<O 0015 to _0 0_Q_5_ -1-2-D-I—chlor-oet-h-ane(I 2-DCA)- ND<O 0015 10 ()00" 11 D14hIoul�thelle ND<O 0015_ 10 f 0 0_0_5- cis-1 2-Dichlotoethene ND<O 0015 10 0 Wis h fns-I 2-D1chloioethene ND<O 0015 l0 0 005 1,2 Dic_hl_oiopropane ND<O 001S 10 0(105 13 Dlchlotupiopinc ND<O 001_5 10 _0 00_5__2 2-Dlchlor_opropane _ ND<O 001 s 10 0 005 I I Dichlor0pt0ptnc ND<0 0015 10_ 0 005 cis-1_3-Dichloropiopene ND<O 0015 10 U O0s cans-1 3-Dlchlmnpiopcne ND<O 0_015_ - 10 0005 Dnsopropy]ether (DIP£_) _ ND<O 001 10 0 00� Lthylbcnzene _ N_D<0 0015 10 0 005 Ethyl tent-butyl ether (ELBE) _____ _ ND<0_001 10 000 f i eon 113 _ �ND<O 030 _E 10 1 0 1 Hexachlorobutadtene 1 ND<0 0015 10 0 OOa I-tekachloroethane _ _ND<0_0_01_5 _ l0_i 0005 2-Hex....e _ __— -ND<0_0015 10 0005 Isoplopylhenzene ND10_<0 0015 1 0 005 __ ro 4-iso 1 toluene- - ND<O 001 S 10 0 005 pY __en_ Mctllyl t-butyl ether (NITBL) ND<0 0015 10 0 005__Methylene chlor_id_e ND<O 0015 10 000S 4 Methyl-2 pent nn 10c(MIBK) ND<O 0015_- 10 - 0005 Naphthalene - _ ND<O 0015 10 000-1 Ntil obenzere ND<O 030 10 0 1 _ n-P1opyl benzene ND<O 0015 10 0 00� 5t�lene ND<O 0015 10 - 0005 _I -T 1 1,2etrachloloetha_ne _ ND<O 0015 10 000 0 1 1 2 2-Tetiachloocthane ND<0 0015 10 005 _Teti achloloeth_ene __ _ ND<O 0015 - IO 0 00-' 10 1 LMIL ND<0 OQ15_ 10 0005 1 2_3-TI ich_loiobenze_ne _ — _ND<O 001 S 10 U 005 1 2 a r1u.h1010ben7ene _ ND<O 001_5_I 10- 0 005 1,1,1-Trichloroethane —_� --ND<O 0015 10 0 005 I 1 2-311chloloethane _ND_<0 00 IS 10 0 005 _Tttchloroethene _ f_ _T _ND<0 0015 10 0 005 f1Ic111o1oilooionlethane _ ND<O 0015 _ 101 0005 1 2 3-Trichlo_topropane ND_<Q 00t9 10 0 005 12 4 Fri nethylbenzene ND<O 0015_ -� -10-�0_005 l 3,5-Tlnnethylben_z_ene_ - ND<O 0015 10 000 Vinyl C 11101 ule ND<O 0015 10 0 005 Xylenes ND<O 001 S 10 0 00"- Surl ogate Recoveries('%1) 82 %5S2 91 ",.SS3 116 C 011111ILMs *\4atca Ind vipoi samples ate Ieporied 111µg/L sorl/sludgelsolld samples In mg/kg,prod uct/arl/non-aqueous liquid samples and all TCLP&SPLP 6\11-lctS ace iepolted In mg/L wipe samples u1)A-,/wipe ND means not detected above the ieporting limit N/A means analyte not applicable to this analysts . iVsuiiog rte diluted nut of range oI coelutes with another peak &)low surrogate due to nlatiixniterfetence h)11=11tu lhan s�rtc 11111misc ibie sheen/product 1s ptesei7t r)liquid sample that contains greater than--1 vol %stdrment,})sdmple diluted clue to high 111 iS1111C LOM LtIl/mall I� Intel tel ence 1.)ieportmg Innit near but 1101 Identical to our standard Ieporting Innit due to variable Encoie simple WClghl 1111 polun� Innu Iarsed due to msuftiClcnt ram le amount n)results ale ieported on a diy weight basis i)see attached narrative DHS Ceitlficatlan No 1644 (M—W(Angela Rydelius, Lab Manager