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08/18/93 15:28 $916 Wl 09.17 JA.NTI RIATONO �'' +-►-+ FALCON 'ERGY X007/007 <br /> Spar r Analytical Laboratory Division <br /> 0 Mobile Laboratory Div<s>ton <br /> Te&mk)gy irt!c. Sc*itfic DMsion <br /> Nth Auromotion rn Mrnd <br /> Metals, CAM 17 Soil <br /> MS / MSD Recoveries <br /> Attention: Mr. Jim Hoblitzell Date Sampled: Aug 10, 1993 <br /> Falcon Energy Date Received: Aug 11, 1993 <br /> P.O. Box 1257 Date Analyzed: Aug 16, 1993 <br /> Stockton, CA 95201 <br /> Project #: 02920 Project Name: Ray Clark <br /> Client ID: MS/MSD LAS ID: ST93-08-016 MS <br /> ST93-08-016 MSD <br /> Matrix: Soil Dilution: <br /> Sample Spike MS % MSD % % <br /> Element Conc. Conc. MS Recovery MSD Recovery RSD <br /> Antimony (Sb) NO 50 NO MI NO MI MI <br /> Arsenic (As) NO 50 NO MI NO Mi MI <br /> Barium (Ba) 200 50 250 100% 240 80% 22% <br /> Beryllium (Be) NO 50 45 90% 41 82% 9% <br /> Cadmium (Cd) NO 50 39 78% 36 72% 8% <br /> Chromium (Cr) 37 50 81 88% 74 74% 17% <br /> Cobalt (Co) 18 50 63 90% 58 80% 12% <br /> Copper (Cu) 30 50 79 98% 74 88% 11% <br /> Lead (Pb) 5.1 50 67 124% 56 102% 20% <br /> Mercury (Hg) 0.046 0.50 0.54 99% 0.57 105% 6% <br /> Molybdenum (Mo) NO 50 30 60% 31 62% 3% <br /> Nickel (Ni) 31 50 79 96% 72 82% 16% <br /> Selenium (Se) NO 50 NO M1 ND MI MI <br /> Silver (Ag) NO 50 49 98% 43 86% 13% <br /> Thallium (Tl) NO 50 ND Ml NO MI MI <br /> Vanadium (V) 58 50 120 104% 100 64% 48% <br /> Zinc (Zn) 61 50 110 98% 100 78% 23% <br /> Nrn—peva PW M"an—mpMp . nwMem per Kiewwn <br /> No -Net Defteew Cempevrtbl may bu puma K ewwo meows bw to fitr— an Nmic <br /> MI = Matrix Interference <br /> Aug 15, 1993 <br /> R. L James.Principal Chemist afar• Reported <br />