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Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 •Sparks,Nevada 89431-5778 <br /> ' (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> Date: OC Summary Report Work Order: <br /> 1741m-08 08060609 <br /> ethod Blank Type MBLK Test Code: EPA Method SW8015 <br /> ile ID: Batch ID:20034 Analysis Date: 06107/2008 15:49 <br /> Sample ID: MBLK-20034 Units: mg/Kg Run ID:FID_2_080606C Prep Date: 06/06/2008 <br /> ■nalyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPORefVal %RPD(Limit) Qual <br /> PH-E (DRO) ND 5 <br /> TPH-E(ORO) NO 10 <br /> aijurr Nonane 67.8 100 68 44 159 <br /> aboratory Control Spike Type LCS Test Code: EPA Method SW8015 <br /> File ID: Batch ID:20034 Analysis Date: 0610712008 16:15 <br /> ample ID: LCS-20034 Units: mg/Kg Run ID:FID_2 080606C Prep Date: 06106/2008 <br /> nalyte Result POL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limit) Qual <br /> PH-E(DRO) 94.7 10 100 95 70 130 <br /> Sun: Nonane 78 100 78 44 159 <br /> ample Matrix Spike Type MS Test Code: EPA Method SW8015 <br /> ile ID: Batch ID:20034 Analysis Date: 061101200810:35 <br /> Sample ID: 08060656-OSAMS Units: mglKg Run ID:FIO_2_080606C Prep Date: 00/06/2008 <br /> Stnalyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPO(Limit) Qual <br /> RPH-E(DRO) 833 10 500 404.4 86 37 164 <br /> um: Nonane 129 100 129 44 159 <br /> ample Matrix Spike Duplicate Type MSD Test Code:EPA Method SW8015 <br /> ile ID: Batch ID:20034 Analysis Date: 08/1012008 11:28 <br /> ample 10: 0806065&05AMSD Units: mg/Kg Run ID:FID_2_080606C Prep Date: 0610612008 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPORefVal %RPD(Limit) Qual <br /> PH-E(DRO) 1080 10 500 404.4 136 37 164 833 26.1(20) R5 <br /> urr: Nonane 131 100 131 44 159 <br /> Comments: <br /> calculations are haled off of raw(non-rounded)data. However.for reporting purposes.all QC dam is rounded to three significant figures.Therefore,hand calculated <br /> lues may differ slightly. <br /> R5=MS/MSD RPD exceed the laboratory control limit. Recovery met acceptance criteria. <br />