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' Alpha Analytical, Inc. <br /> ' 255 Glendale Ave.•Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> Date: QC Summary Report Work 13091703r <br /> I7-Seo-13 <br /> Method Blank Type MBLK Test Code:EPA Method SW8015B1C Ext <br /> ' File ID:7A09171362.D Batch ID:31665 Analysis Date: 091181201316:50 <br /> Sample ID: MBLK-31665 Units:mg1L Run ID:FID_7_130918A Prep Date: 091181201310:38 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> TPH-E(DRO) ND 0.5 <br /> Sur.Nonane 0.174 0.15 116 53 145 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW801581C Ext <br /> File ID:7A09171363.D Batch ID:31665 Analysis Date: 09/181201317:18 <br /> ' Sample ID: LCS-31665 Units: molt. Run ID:FID_7_130918A Prep Date: 091181201310:38 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qua] <br /> TPH-E(DRO) 2.6 0.05 2.5 104 70 130 <br /> Sum.Nonane 0.182 0.15 121 53 145 <br /> ' Sample Matrix Spike Type MS Test Gode: EPA Method SW8015BIC Ext <br /> File ID:7A09171382.D Batch ID:31665 Analysis Date: 09119/2013 01:45 <br /> Sample ID: 13091703-IBAMS Units: mg1L Run ID:FID_7_13091&A Prep Date: 091181201310:38 <br /> ' Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> TPH-E(DRO) 13.2 0.05 2.5 10.42 110 51 151 <br /> Sum:Nonan 0.201 0.15 134 53 145 <br /> Sample Matrix Spike Duplicate Type MSD Test Code:EPA Method SW801581C Ext <br /> File ID:7A09171383.D Batch ID:31665 Analysis Date: 0911912013 02:12 <br /> Sample ID: 13091703-ISAMSD Units:mg1L Run ID:FID_7_130918A Prep Date: 091181201310:38 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Llmit) Qual <br /> ' TPH-E(DRO) 15.4 0.05 2.5 10.42 198 51 151 13.18 15.4(40) M3 <br /> Sum:Nonane 0.159 0.15 106 53 145 <br /> Comments: <br /> Calculations are based off of raw(non-roundod)data.However,for reporting purposes,all QC data is rounded to three significant figures.'lberefore,hand calculated <br /> ' values may differ slightly. <br /> M3=The accuracy of the spike recovery value is reduced since the analyte concentration in the sample is disproportionate to the spike level.The method control <br /> sample recovery was acceptable. <br /> 1 <br />