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ENVIRONMENTAL <br /> Analytical Chemists <br /> September 19, 1996 RE: Organic Analyses Lab # STK 634719 <br /> San Joaquin County Solid Waste Sampling Site: Corrol Hollow Landfill UST <br /> C/O S. J. Co Purchasing-Mike Selling <br /> P.O. Box 1810 <br /> Stockton , CA 95201 <br /> Sample Handling Information <br /> Sample Batch Sample Sample Grab or Sampled Date Samp. Container <br /> ID Number ID Description Type Comp. by Sampled Received Extracted Analyzed & Preservatives <br /> 1 STK960917-00 A QA/QC Blank --- N/A 09/17/% <br /> 2 STK634719-01 A N. Wall 14.5' down Soil Grab Brian Pabst 09/10/% 09/10/96 N/A 09/17/96 1,a <br /> 3 STK634719-02 A Bottom Center 16.51 down Soil Grab Brian Pabst 09/10/96 09/10/96 N/A 09/17/96 l,a <br /> 4 STK634719-03 A S.W. Corder 12.51 dorsi Soil Grab Brian Pabst 09/10/96 09/10/96 N/A 09/17/96 1,a <br /> 5 STK634719-04 A Composite North Piles A,B,C,D Soil Camp. Brian Pabst 09/10/96 09/10/96 N/A 09/17/96 1,a <br /> 6 STK634719-05 A Composite-South Piles A,B,C,D Soil Camp. Brian Pabst 09/10/96 09/10/96 N/A 09/17/96 1,a <br /> Preservatives: (1) Cool 4°C Containers: (a) Glass Jar <br /> ANALYTICAL RESULTS <br /> Ethyl <br /> Sample BFB Benzene Benzene Methyl tent-Butyl Ethe Toluene Xylene <br /> ID Description % Rec. DLR RESULT DLR RESULT DLR RESULT DLR RESULT DLR RESULT <br /> 1 QA/QC Blank - STK96091700L A 124 0.3 ND 0.3 MD 5 ND 0.3 ND 0.3 ND <br /> 2 N. Wall 14.51 down 111 0.003 MD 0.003 ND 0.020 ND 0.003 ND 0.003 ND <br /> 3 Bottom Center 16.5' down 110 0.003 ND 0.003 MD 0.020 ND 0.003 ND 0.003 ND <br /> 4 S.W. Corner 12.51 down 105 0.003 ND 0.003 ND 0.020 ND 0.003 ND 0.003 ND <br /> 5 Composite North Piles A,B,C,D 102 0.003 ND 0.003 ND 0.020 IID 0.003 ND 0.003 ND <br /> 6 Composite-South Piles A,B,C,D 79 0.003 ND 0.003 ND 0.020 ND 0.003 ND 0.003 ND <br /> Units Surrogate m9/K9 mg/Kg mg/K9 mg/Kg mg/Kg <br /> Analytical Method AR (%) EPA 8020 EPA 8020 EPA 8020 EPA 8020 EPA 8020 <br /> Acceptable Range 75-125 <br /> ND = Not Detected at or above the Detection Limit Reported (DLR). ♦ = DLR adjusted because of dilutions, concentrations, or limited sample. <br /> Please see next page for comments . . . <br /> norate OflirA�&Laboratory Office 8 Laboratory Field Office <br /> P.O.Box 272 Corporation Street 2500 Starh RVisal' lilornia <br /> Santa Paula 1-0272 Stockton, �15 TEL. 7349473 <br /> J// T Whiirfff11191 717 11go <br />