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1 Alpha Analytical, Inc. 255 Glendale Ave - Suite 21 • Sparks,Nevada 89431-5778 (775) 355-1044 •(775) 355-0406 FAX • 1-800-283-1183 Date QC Summary Report Work Order ' 2)-Apr-03 03041422 Sample Matrix Spike Type MS Test Code EPA Method SW8260B File ID D IMSDCHEMIMS121DATA1030416k03041609 D Batch ID MS12SO415A Analysis Date 04/16/2003 11 40 ' Sample ID 03041422-03AMS Units pg/Kg Run ID GCIMSD_12_030415B Prep Date 04!1412003 Analyte Result PQL SpkVal SpkRefVal %REC LoWLimft Hight.tmit RPD Ref Val %RPD Quaff 11-Dichloroethene 206 20 200 0 103 0 148 ' Benzene 204 5 200 0 102 32 148 Trichloroethene 199 20 200 0 99 17 177 Toluene 219 5 200 0 110 39 136 Chlorobenzene 220 20 200 0 110 27 162 Ethylbenzene 229 5 200 0 115 45 152 m p-Xylene 455 5 400 0 114 42 154 o-Xylene 238 5 200 0 119 41 154 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B ' File lD D IMSDCHEMIMS12kDATA1030416k03041610 D Batch lD—MS12SO415A Analysis Date 04/16/2003 12 01 Sample ID 03041422-03AMSD Units pg/Kg Run lD GCIMSD 12 0304156 Prep Date 0411412003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighUrrut RPD Ref Val %RPD Qual ' 1 1-Dichloroethene 210 20 200 0 105 0 148 2055 202 Benzene 202 5 200 0 101 32 148 2044 124 Trichloroethene 197 20 200 0 99 17 177 1988 0 702 Toluene 212 5 200 0 106 39 136 2191 3 37 Chlorobenzene 212 20 200 0 106 27 162 2197 361 Ethylbenzene 225 5 200 0 113 45 152 2292 162 m p-Xylene 447 5 400 0 112 42 154 4551 1 89 o-Xylene 229 5 200 0 115 41 154 2379 372 jWments. ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix B-Analyte detected in the associated Method Blank I ' I I i i