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I <br /> Alpha Analytical, Inc. <br /> 255 Glendale Ave •Suite 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX • 1-800-283-1183 <br /> �A1e t OC Summary Report Work Order!{-Apr-03 03040601 <br /> Sample Matrix Spike <br /> Type MS Test Code EPA Method SW8260B <br /> File ID D 1HPCHEM1MS09kDATA1030407k03040713 D Batch ID MS9SO407A Analysis Date 04/07/2003 13 34 <br /> Sample ID 03040201-20AMS Units pg/Kg Run ID GCIMSD_9�030407A Prep Date 04104/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowbmit HighLimit RPD Ret Val %RPD Qual <br /> 11-Dichloroethene 114 20 200 0 57 0 148 <br /> Benzene 160 5 200 0 80 32 148 <br /> ' Trnchloraethene 159 20 200 0 79 17 177 <br /> Toluene 169 5 200 0 84 39 136 <br /> Chlorobenzene 174 20 200 0 87 27 162 <br /> Ethylbenzene 177 5 200 0 88 45 152 <br /> ' m p-Xylene 335 5 400 0 84 42 154 <br /> o-Xytene 171 5 200 0 85 41 154 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B <br /> ' File ID D XHPCHEMXMS09kDATAk03O4O7103040714 D Batch ID+MS9SO407A Analysis Date 04/07/2003 13 58 <br /> Sample 1D 03040201-20AMSD Units pg/Kg Run ID GCIMSD 9 030407A Prep Date 04/04/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imlt HighLimit RPD Ref Vat %RPD Qual <br /> 1 1-Dichloroethene 785 20 200 0 39 0 148 114 368 <br /> Benzene 114 5 200 0 57 32 148 1603 342 <br /> Trichloroethene 114 20 200 0 57 17 177 1585 328 <br /> Toluene 118 5 200 0 59 39 136 1685 35 <br /> Chlorobenzene 123 20 200 0 61 27 162 1738 34 4 <br /> ' Ethylbenzene 125 5 200 0 62 45 152 1766 344 <br /> m p-Xylene 239 5 400 0 60 42 154 3347 336 <br /> o-Xylene 121 5 200 0 61 41 154 1706 338 <br /> Ornments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated <br /> S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limtts due to matrix <br /> B-Analyte detected in the associated Method Blank <br /> I <br /> 1 <br /> 1 <br /> I <br />