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Alpha Analytical, Inc. 255 Glendale Ave •Suite 21 • Sparks,Nevada 89431-5778 (775)355-1044 •(775)355-0406 FAX• 1-800-283-1183 i IOU rte QC Summary Report Work Order ' 14-Apr-03 03040601 Sample Matrix Spike Type MS Test Code EPA Method SW8260B File ID D IHPCHEMIMS101DATA1030407103040713 D Batch ID MSi0W0407A Analysis Date 04/0712003 12 21 ' Sample ID 03040601-02AMS Units pg1L Run ID GCIMSD_10_030407A Prep Date 04/0712003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual 1 1-Dichloroethene 518 25 50 0 104 80 120 ' Benzene 509 1 3 50 0 102 80 120 Trichloroethene 514 25 50 3 12 97 62 137 Toluene 478 1 3 50 0 96 80 120 Chlorobenzene 486 2 5 50 0 97 80 121 Ethylbenzene 501 13 50 0 100 80 120 m p-Xylene 945 1 3 100 0 95 73 129 o-Xylene 486 1 3 50 0 97 73 127 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B ' File ID D IHPCHEMIMS101DATA1030407103040714 D Batch iD MS10W0407A Analysis Date 04/0712003 12 42 Sample ID 03040601-02AMSD Units ligIL Run lD GCIMSD_10_030407A Prep Date 04/07/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imd RPD Ref Val %RPD Qual ' 1 1-Dichloroethene 533 2 5 50 0 107 80 120 5184 276 Benzene 512 13 50 0 102 80 120 509 0 529 Trichloroethene 537 2 5 50 3 12 101 62 137 5144 4 55 Toluene 499 13 50 0 998 80 120 4776 44 Chlorobenzene 497 2 5 50 0 99 80 121 4855 242 ' Ethylbenzene 506 1 3 50 0 101 80 120 501 1 03 m,p-Xylene 964 1 3 100 0 96 73 129 94 52 1 97 o-Xylene 483 1 3 50 0 97 73 127 4857 0 537 mments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matnx B-Analyte detected to the associated Method Blank 1