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Alpha Analytical, Inc. 255 Glendale Ave •Sutte 21 •Sparks,Nevada 89431-5778 (775)355-1044 •(775)355-0406 FAX• 1-800-283-1183 ate' QC Summary Report Work Order 25 Apr 03 03041422 Method Blank Type MBLK Test Code EPA Method SW8015 Pile ID D IMSDCHEMIMS121DATA1030416103041607 D Batch ID MS12SO415B Analysis Date 04/1612003 10 59 ' Sample ID MBLKMS12SO415A Units mg/Kg Run ID GC/MSD-12-030415B Prep Date 04/16/2003 Analyte Result PQL SpkVal SpkReNal %REC Lowt-imit HighLimit RPD Ref Val %RPD Qual TPH Purgeable NO 1 ' Laboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID D 1MSDCHEM1MS121DATA1030416103041611 D Batch ID MS12SO415B Analysis Date 0411612003 12 24 Sample ID GLCSMS12SO4158 Units mg/Kg Run ID GCIMSD_12_03041513 Prep Date 04/16/2003 ' Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual TPH Purgeable 682 1 8 85 61 144 Sample Matrix Spike Type MS Test Code EPA Method SW8015 ' File ID D 1MSDCHEM1MS121DATA1030416103041612 D Batch ID MS12SO415B Analysis Date 04116/2003 12 45 Sample 0 03041422.03AGS Units mg/Kg Run ID GCIMSD_12_030415B Prep Date 0411612003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual ' TPH Purgeable 6 11 1 8 0 76 61 144 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8015 File ID D 1MSDCHEM1MS121DATA1030416103041613 D Batch ID MS12SO415B Analysis Date 04/16/2003 13 06 ' Sample ID 03041422-03AGSD Units mg1Kg Run ID GCIMSD_12_030415B Prep Date 04116/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imitHighLimit RPD Ref Val %RPD Qual TPH Purgeable 592 1 8 0 74 61 144 6 112 3 26 wments ND Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix B-Analyte detected in the associated Method Blank 1 1 I i