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Sequoia 1455 McDowell Blvd North Ste D <br /> Petaluma CA 94954 <br /> 1! 4 (707) 792-1865 <br /> - Analytical FAX(707) 792-03.42 <br /> I168 <br /> ne Technical Services,Inc Project Shell Oil Co Sampled 2/11/99 <br /> 0 Rogers Ave Project Number 1267 Country C1ub,Stockton/990211-K2 Received 2/16/99 <br /> Jose,CA 95112 Project Manager Ann Pember Reported 4/9/99 <br /> Total Petroleum Hydrocarbons as Diesel&others by EPA 8015M/Quality Control <br /> Sequoia Analytical-Petaluma <br /> Date Spike Sample QC Reporting Limit Recov RPD RPD <br /> Analyte Analyzed Level Result Result Units Recov Limits % Limit % Notes* <br /> Batch 9020456 Date Prepared_ 2/20/99 Extraction Method EPA 3520B <br /> Blank 9020456-BLKl <br /> Diesel 3/3/99 00666 mg/1 00500 6 <br /> Surrogate o-Terphenyl N 0 100 00677 677 <br /> LCS 9020456-BS1 <br /> Diesel 3/3/99 1 00 0 672 mg/I 280-138 672 <br /> Surrogate o-Terphenyl Pr0100 00851 851 <br /> LCS Dun 9020456-BSD1 <br /> Diesel 3/3/99 1 00 0 740 mg/1 290-138 740 963 <br /> Surrogate o-Terphenyl 0 100 00917 91 7 <br /> uoia Analytical-Petaluma *Refer to end of report for text of notes and definitions <br /> AM 0 v <br /> Page 9 of 11 <br />