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Sequoia 6110 Chesapeake Drive Redwood City,CA 94063 (650)364-9600 FAX(650)364-9233 <br /> 404 N.Wiget Lane Walnut Creek,CA 94598 (925)988-9600 FAX(925)988-9673 <br /> III Striker Avenue,Suite 8 Sacramento,CA 95834 (916)921-9600 FAX(916)921-0100 <br /> Analytical 1455 McDowell Blvd,North,Ste.D Petaluma,CA 94954 (707)792-[865 FAX(707)792-0342 <br /> .......... <br /> ............. <br /> E -X <br /> Blaine T <br /> ech Services, Inc. Client Project ID: She'll 112-67 Country Club <br /> 1680 Rogers Ave. Matrix: Liquid <br /> .".San Jose, CA 95112 <br /> Attention: Fran Thie Work Order#: 9808957 01, 03-06 <br /> Reported: Sep 9, 1998.,- <br /> Ei. <br /> 9808961 07 <br /> QUALITY CONTROL DATA REPORT <br /> Analyte: Methanol <br /> QC Batch#: GCO818981SHSHSB <br /> Analy.. Method: ISH8 li <br /> Prep. Method: HS <br /> Analyst: T.Sorokin <br /> MS/MSD#: 980890303 <br /> Sample Cone.: N.D. <br /> Prepared Date: 8/17/98 <br /> Analyzed Date: 8/17/98 II <br /> Instrument I.D.#.* GCv1 <br /> Cone. Spiked: 8.0 mg/L <br /> Result: 7.9 <br /> MS % Recovery: 99 <br /> Dup. Result: 7.3 <br /> MSD %Recov.: 91 <br /> RPD: 7.9 <br /> RPD Limit: 0-50 <br /> ........ ..... <br /> .............. <br /> ............ <br /> ... ........................ ... ..... ..................................................... .... <br /> .......... <br /> ................... ............ <br /> ..---- <br /> ............................ ............................. . ......................................... <br /> LCS#: LCS081898 <br /> Prepared Date: 8/18/98 <br /> Analyzed Date: 8/18/98 <br /> Instrument I.D.#: GCV1 <br /> Cone. Spiked: 8.0 mg/L <br /> LCS Result: 6.8 <br /> LCS % Recov.: 85 <br /> MS/MSD <br /> LCS; <br /> Control Limits 70-130 <br /> Please Note: <br /> The LCS is a control sample of known,interferent-free matrix that is analyzed using the same reagents, <br /> SE A A ALYTICAL preparation,and analytical methods employed for the samples. The matrix spike is an aliquot of sample <br /> fortified with known quantities of specific compounds and subjected to the entire analytical procedure, If <br /> the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br /> interference,the LCS recovery is to be used to validate the batch. <br /> eg gy nner <br /> rojec anager MS=Matrix Spike,MSD=MS Duplicate,RPD=Relative%Difference 9808957.BLA <1> <br /> 4 <br />