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Sequoia 680 Chesapeake Dnve Redwood City,CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 404 N Wiget Lane Walnut Creek,CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> frala� Analytical 819 Striker Avenue,Suite 8 Sacramento,CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> Envlros Client Prol ID Shell 1267 Country Club, Stck Sampled 04/04/97 <br /> 270 Perkins Ave Sample Descript SB-2-6 Received 04/08/97 <br /> Sonoma, CA 95476 Matrix SOLID Extracted 04/17/97 <br /> Analysis Method EPA 8270 Analyzed 04/18/97 <br /> Attention Joe Neely Lab Number 9704512-04 Reported 04f22j97 <br />)C Batch Number MSO414978270EXA <br /> nstrument ID F4 <br /> Analyte Detection Limit Sample Results <br /> ug/Kg ug/Kg <br /> Di-n-octyl phthalate 250 N D <br /> Fluoranthene 250 N D <br /> Fluorene 250 N D <br /> Hexachlorobenzene 250 N D <br /> Hexachlorobutadiene 250 N D <br /> H exachl orocycl a pentad i ene 500 N D <br /> Hexachloroethane 250 N D <br /> 1ndeno(1,2,3-cd)pyre ne 250 N D <br /> Isophorone 250 N D <br /> 2-Methylnaphthalene 250 N D <br /> 2-Methylphenol 250 N D <br /> 4-Methylphenol 250 N D <br /> Naphthalene 250 N D <br /> troaniline 500 <br /> troanillne 500 N D <br /> iD <br /> 4-Nitroaniline 500 N D <br /> Nitrobenzene 250 N D <br /> 2-Nitrophenol 250 N D <br /> 4-Nitrophenol 500 N D <br /> N-Nitrosodiphenylamine 250 N D <br /> N-Nitroso-di-n-propylamine 250 N D <br /> Pentachlorophenol 500 N D <br /> Phenanthrene 250 N D <br /> P 250 770 <br /> Phenol <br /> P 250 N D <br /> Pyrene <br /> 1,2,4-Trichlorobenzene 250 N D <br /> 2,4,5-Trichlorophenol 500 N D <br /> 2,4,6-Trichlorophenol 250 N D <br /> Surrogates Control Limits% % Recovery <br /> 2-Fluorophenol 25 121 68 <br /> Phenol-d5 24 113 67 <br /> Nitrobenzene-d5 23 120 55 <br /> 2-Fluorobiphenyl 30 115 53 <br /> 2,4,6-Tribromophenol 19 122 65 <br /> p-Terphenyl-d14 18 137 59 <br /> Analytes reported as N D were not present above the stated limit of detection <br /> SEQUOIA ANALYTICAL - ELAP #1210 <br /> Mike reg ry <br /> Project Manager Page 7 <br /> r� - <br />