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Sequoia 680 Chesapeake Drive Redwood City,CA 94063 (415) 364 9600 FAX(415) 364 9233 <br /> 4 15) <br /> 404 N Wiget Lane Walnut Creek, CA 94598 (510) 988 9600 FAX(510)988 9673 <br /> 1I) Analytical 819 Striker Avenue,Suite 9 Sacramento,CA 95834 (916) 921 9600 FAX(916)921 0100 <br /> 0 <br /> Enviros - Client Proj ID Shell 1267 Country Club, Stck Sampled 04/04/97 <br /> 270 Perkins Ave Sample Descrlpt SB-2-11 Received 04/D8/97 <br /> Sonoma, CA 95476 Matrix SOLID Extracted 04/17/97 <br /> Analysis Method EPA 8270 Analyzed 04/18/97 <br /> Attention Joe Neely Lab Number 9704512-05 Reported 04f22197 <br />)C Batch Number MSO414978270EXA <br /> istrument ID F4 <br /> Analyte Detection Limit Sample Results <br /> ug/Kg ug/K9 <br /> Dl-n-octyl phthalate 250 N D <br /> Fluoranthene 250 N D <br /> Fluorene 250 N D <br /> Hexachlorobenzene 250 N D <br /> Hexachlorobutadiene 250 N D <br /> Hexachlorocyclopentadiene 500 N D <br /> Hexachloroethane 250 N D <br /> lndeno(1,2,3-cd)pyrene 250 N D <br /> Isophorone 250 N D <br /> 2-Methylnaphthalene 250 N D <br /> 2-Methylphenol 250 N D <br /> 4-Methylphenol 250 N D <br /> Naphthalene 250 N D <br /> troandlne 500 N D <br /> roaniline 500 N D <br /> 4- itroaniline 500 N D <br /> Nitrobenzene 250 N D <br /> 2-Nitrophenol 250 N D <br /> 4-Nitrophenol 500 N D <br /> N-Nitrosodiphenylamine 250 <br /> N-Nitroso-dl-n-propylamine 250 N D <br /> Pentachlorophenol 500 N D <br /> Phenanthrene 250 N D <br /> Phenol 250 930 <br /> Pyrene 250 N D <br /> 1,2,4-Trlchlorobenzene 250 N D <br /> 2,4,5-Trichlorophenol 500 N D <br /> 2,4,6-Trichiorophenol 250 N D <br /> Surrogates Control Limits% % Recovery <br /> 2-Fluorophenol 25 121 60 <br /> Phenol-d5 24 113 59 <br /> Nitrobenzene-d5 23 120 48 <br /> 2-Fluorobiphenyl 30 115 48 <br /> 2,4,6-Tribromophenol 19 122 52 <br /> p-Terphenyl-d14 18 137 52 <br /> Analytes reported as N D were not present above the stated limit of detection <br /> SEQUOIA ANALYTICAL - ELAP #1210 <br /> Mia Gregory <br /> Project Manager Page t2 <br />