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Sequoia 680 Chesapeake Redwood Cary,CA 94063 (415) 364 9600 FAX(41 ) 364 9633 <br /> 404 N Wiget Lanene Walnut Creek, CA 94598 (510) 989 9600 FAX(5100) 988 9673 <br /> ue,Suite B Sacramento,CA 95834 (916) 921 9600 FAX (916)921 0100 <br /> Analytical 819 Striker Aven <br /> Enviros Client Prof ID Shell 1267 Country Club, Stck Sampled 04/04/97 <br /> 270 Perkins Ave Sample Descript SB-2-Liq Received 04/08/97 <br /> Sonoma, CA 95476 Matrix LIQUID Extracted 04/11/97 <br /> Analysis Method EPA 8270 Analyzed 04/17/97 <br /> Attention Joe Neely Lab Number 9704512-10 Reported 04122197 <br /> QC Batch Number MSO410978270EXA <br /> Instrument ID F4 <br /> Analyte Detection Limit Sample Results <br /> ug/L. u9/L <br /> Di-n-octyl phthalate 10 N D <br /> Fluoranthene 10 N D <br /> Fluorene 10 N D <br /> Hexachiorobenzene 10 N D <br /> Hexachlorobutadiene 10 N D <br /> Hexachlorocyclopentadiene 20 N D <br /> Hexachloroethane 10 N D <br /> lndeno(1,2,3-cd)pyrene 10 N D <br /> Isophorone 10 N D <br /> 2-Methylnaphthalene 10 390 <br /> 2-Methylphenol 10 N D <br /> 4-Methylphenol 10 N D <br /> Naphthalene 10 350 <br /> itroaniline 20 N D <br /> itroaniline 20 N D <br /> itroaniline 20 ND <br /> Nitrobenzene 10 ND <br /> 2-Nitrophenol 10 ND <br /> N D <br /> 4-Nitrophenol 20 N D <br /> n-Nitrosodiphenylamine 10 <br /> n-Nitroso-di-n-propylamine 10 ND <br /> Pentachiorophenol 20 ND <br /> Phenanthrene 10 ND <br /> Phenol 10 ND <br /> Pyrene 1dN D <br /> 1,2,4-Trichlorobenzene 10 <br /> 2,4,5-Trichlorophenol 20 ND <br /> 2,4,6-Trichlorophenol 10 ND <br /> Surrogates Control Limits% % Recovery <br /> 2-Fluorophenol 21 110 32 <br /> Phenol-d5 10 110 39 <br /> Nitrobenzene-d5 35 114 58 <br /> 2-Fluorobiphenyl 43 116 76 <br /> 2,4,6-Tribromophenol 10 123 107 <br /> p-Terphenyl-d14 33 141 74 <br /> Analytes reported as N D were not present above the stated limit of detection <br /> SEQUOIA ANALYTICAL - ELAP #1210 <br /> M r ory <br /> Page 26 <br /> Project Manager <br />