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Report Number: 30756 II Date . 1/10/2003 QC Report : Matrix Spike/Matrix Spike Duplicate Project Name : 1267 Country Club Project Number: 030103-SH-1 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup. Valuer! Samplelue Units Method Araial ed Percent oRecov t DEff nt Rani{v• emit Parameter Sample Value Le TPH as Diesel Blank <50 1000 1000 892 869 ug/L M EPA 8015 118103 89.2 86.9 2.68 70-130 25 Benzene 30753-07 <0.50 38.4 38.8 39.0 38.8 ug/L EPA 82608 119103 102 100 1.51 70-130 25 Toluene 30753-07 <0.50 38.4 38.8 40.1 39.7 ug/L EPA 8260B 119/03 104 102 2.01 70-130 25 Tert-Butanol 30753-07 <5.0 192 194 196 193 ug/L EPA 8260B 1/9103 102 99.5 2.40 70-130 25 Methyl-t-Butyl Ether 30753-07 1.1 38.4 38.8 37.6 37.5 ug/L EPA 82606 119103 95.0 93.9 1.21 70-130 25 Benzene 30747-05 <0.50 40.0 40.0 39.6 39.2 ug/L EPA 8260B 118103 99.0 98.1 0.888 70-130 25 Toluene 30747-05 <0.50 40.0 40.0 37.6 37.9 ug/L EPA 82606 118103 94.0 94.8 0.901 70-130 25 Tert-Butanol 30747-05 <5.0 200 200 196 192 ug/L EPA 82606 118103 97.8 95.8 2.04 70-130 25 Methyl-t-Butyl Ether 30747-05 170 40.0 40.0 222 224 ug/L EPA 82608 118103 140 144 2.66 70-130 25 Benzene 30756-01 34 40.0 40.0 71.2 70.6 ug/L EPA 82608 118103 92.2 90.7 1.72 70-130 25 Toluene 30756-01 1.7 40.0 40.0 38.9 39.0 ug/L EPA 8260B 118103 93.0 93.3 0.295 70-130 25 Tert-Butanol 30756-01 6.4 200 200 200 204 ug/L EPA 8260B 1/8103 96.6 8 2.28 1 AO 70-130 25 70-130 25 Methyl-t-Butyl Ether 30756-01 <0,50 40.0 40.0 35.7 36.0 ug/L EPA 82608 118103 89.2 90. II Approved By: J I Kiff KIFF ANA CAL, LLC • 2795 2nd St Suite 300 vis, CA 95.616 530-297-4800