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819 SenAve Ste Sequoia Sacramentoto CA 958344 (916)921-9600 iW Analytical FAX(916)921-0100 www sequoialabs corn ettler-Ryan-Petaluma Project Tosco 11192,Stockton,CA 5212209 1364 N McDowell Blvd Ste B2 Project Number NIA Reported Petaluma CA,94954 Project Manager Dave Vossler 12/31/02 11 16 Notes and Definitions E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument HT-RS This sample was originally analyzed within the EPA recommended hold time Re-analysts for confirmation or dilution was performed past the recommended hold time The results may still be useful for their intended purpose Q-28 The opening calibration verification standard was outside acceptance limits by-1% Although the Laboratory Control Sample verified the accuracy of the batch,this should be considered in evaluating the data for its intended purpose Q-28a The opening calibration verification standard was outside acceptance limits by-2% Although the Laboratory Control Sample verified the accuracy of the batch,this should be considered in evaluating the data for its intended purpose Q-28b The opening calibration verification standard was outside acceptance lrnvts by-6% Although the Laboratory Control Sample venfied the accuracy of the hatch,this should be considered in evaluating the data for its intended purpose Q-Lllvl The percent recovery was outside of the control limits The samples results may still be useful for their intended purpose DET Analyte DETECTED ND Analyte NOT DETECTED at or above the reporting limit i NR Not Reported dry Sample results reported on a dry weight basis RPD Relative Percent Difference Cluoia Analytical -Sacramento The results in this report apply to the samples analyzed in accordance with the chain of custody document Unless otherwise stated results are reported on a wet weight basis This analytical report must be reproduced in its entirety Page 13 of 13 I