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STLSubmission# 2004-05-0866 <br /> Gas/BTEX Fuel Oxygenates by 8260B <br /> TRC Alton Geoscience <br /> Attn AnJu Farfan <br /> 21 Technology Drive <br /> Irvine, CA 92718 <br /> Phone (949)341-7440 Fax (949)753-0111 <br /> Project 41050001 FA20 Received 05/24/2004 11 50 <br /> Conoco Phillips# 11192 <br /> Site 1403 Country Club Blvd, Stockton <br /> Batch CIC Report <br /> Prep(s) 5030B Test(s) 8280FAB <br /> Matrix Spike (MS 1 MSD J Water QC Batch#2004f06103.2B 66 <br /> MW-5 »NIS Lab ID 2004-05a)860,-008 <br /> MS 2004106103,28 66-010 Extracted 06/03/2004 Analyzed 06/03/2004 22 10 <br /> Dilution _ - - ----100- <br /> MSD` 2004106103-28 66-934 Extracted 08103/2004 Analyzed 0610312004 22,34 <br /> Dilution 100 <br /> Compound Conc u Spk Level Recovery% Limits% Isla s <br /> MS MSD Sample u 1L MS MSD RPD Ree RPD MS MSD <br /> Methyl Cert-butyl ether 230 235 0 578 25 921 917 04 65-165 20 <br /> Benzene 219 248 ND 25 876 992 124 69129 20 <br /> Toluene 229 240 ND 25 916 960 4 7 70-130 20 <br /> Surrogate(s) <br /> 1,2-Drchloroethane-d4 527 512 500 1054 1024 72-128 <br /> Toluene-d8 533 531 1 500 1106 S 1106 2 1 180-113 <br /> Severn Trent Laboratories, Inc 06/07/2004 18 04 <br /> STL San Francisco-1220 Quarry Lane,Pleasanton,CA 94566 <br /> A parta8mm Tent Plc Tel 925 484 1919 Fax 925 484 1096 1 www stl-Inc cam•CA DHS FLAP#2496 Page 18 of 19 <br />