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Submission 2005-03-0010 <br /> • Volatile Organic Compounds by 8260B <br /> TRC Afton Geoscience- Irvine <br /> Attn Anlu Farfan <br /> 21 Technology Drive <br /> Irvine, CA 92718 <br /> Phone (949) 341-7440 Fax (949) 753-0111 <br /> Project 41050001 FA20 Received 02/28/2005 15 05 <br /> Conoco Phillips# 11192 <br /> Site 1403 Country Club Blvd Stockton <br /> Batch QC Report <br /> Prep(s) 50308 Test(s) 82608 <br /> Matrix Spike( MS 1 MSD ) Water QC Batch #2005103111-1A 06 <br /> MS/MSD Lab ID 2005-03-0077 -001 <br /> MS 2005103111-1A 06-008 Extracted 03/11/2005 Analyzed 03/11/2005 15 10 <br /> Dilution 4000 <br /> MSD 2005/03111-1A 06-009 Extracted 03/11/2005 Analyzed 03/11/2005 15 46 <br /> Dilution 4000 <br /> Compound Conc ug IL Spk Level Recove % Limits% Fla s <br /> MS MSD Sample u /L MS MSD RPD Rec RPD MS MSD <br /> Benzene 786 783 0 654 800 982 978 0 4 69-129 20 <br /> Chlorobenzene 758 753 0 939 800 946 94 0 0 6 61-121 20 <br /> 1 1-Dichloroethene 798 777 ND 800 998 971 2 7 65-125 20 <br /> Toluene 774 765 0 603 800 967 955 1 2 70-130 20 <br /> Trichloroethene 778 762 3 58 800 968 94 8 21 74-134 20 <br /> Surrogate(s) <br /> 4-Bromofluorobenzene 471 463 500 94 2 926 79-118 <br /> 1 2-Dichloroethane-d4 469 466 500 937 932 78-117 <br /> Toluene-d8 464 448 500 92 8 89 6 77-121 <br /> Severn Trent Laboratories, Inc 03/15/2005 13 21 <br /> STL San Francisco* 1220 Quarry Lane Pleasanton CA 94566 <br /> A part of Seem Trent Plc Tel 925 484 1919 Fax 925 484 1 096*www stl-enc cam*CA DHS ELAP#2496 Page 6 of 7 <br />