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STLSubmission 2005-03-0110 <br /> Gas/BTEX Fuel Oxygenates by 8260B <br /> SECOR-Sacramento <br /> Attn Amy Draffan <br /> 3017 Kilgore Road, Suite 100 <br /> Rancho Cordova, CA 95670 <br /> Phone (916) 861-0400 Fax (916) 861-0430 <br /> Project 77CP 60004 01 0192 Received 03/02/2005 16 00 <br /> Conoco Philips Site# 11192 <br /> Site 1403 Country Club Dr, Stockton, CA <br /> Batch QC Report <br /> Prep(s) 50306 Test(s) 82608 <br /> Matrix Spike ( MS!MSD ) Water QC Batch #2005103!09-2C 68 <br /> MS/MSD Lab ID 2005-03-0264 - 006 <br /> MS 2005/03/09-2C 68-056 Extracted 03/09/2005 Analyzed 03/09/2005 19 56 <br /> Dilution 1 00 <br /> MSD 2005103109-2C 68-014 Extracted 03/09/2005 Analyzed 03/09/2005 20 14 <br /> Dilution 1 00 <br /> Compound Conc ug IL S k Leve Recove % Limits% Flags <br /> MS MSD Sample u IL MS MSD RPD Rec RPD MS MSD <br /> Methyl tert-butyl ether 285 227 ND 25 1140 908 227 65-165 20 R1 <br /> Benzene 265 226 ND 25 106 0 904 159 69-129 20 <br /> Toluene 268 234 ND 25 1072 936 135 70-130 20 <br /> Surrogate(s) <br /> 1 2-Dichloroethane-d4 446 434 500 892 868 73-130 <br /> Toluene-d8 500 499 500 1 1000 9913 81-114 <br /> Severn Trent Laboratories, Inc 03/16/2005 16 06 <br /> STL San Francisco' 1220 Quarry Lane Pleasanton CA 94566 <br /> A part of Severn Trent Plc Tel 925 484 1919 Fax 925 484 1096`www stl-enc com'CA DHS ELAP#2496 Page 8 of 10 <br />