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110 2nd Avenue South,#D7 Pacheco CA=5560F4McCamrbell Analytical Inc Telephone 925-798-1620 Fax 925-hap//wwwmica bellcoin Email main <br /> ' Advanced GeoEnvironmental, Inc Client Project ID Country Club Food& Date Sampled 11/21/02 <br /> Fuel <br /> $37 Shaw Road Date Received 11/22/02 <br /> Client Contact Paul Dotson Date Extracted 11/25/02-11126/02 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 11/25/02-11/26/02 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0211391 <br /> Lab ID 0211391-001C 0211391-002C 0211391-003C 0211391-004C <br /> Client ID MW1/11-21-02 MW2/11-21-02 MW3/11-21-02 1 MW4/11-21-02 Reporting Limttfor <br /> ' Matrix - W -- ---- W ---I----- W - W DF=l <br /> DF 25 1 1 1 S W <br /> 3 <br /> Compound Concentration ug/kg µg1L <br /> tert-Amyl methyl ether(TAME) ND<12 ND ND ND NA 05 <br /> ' Benzene ND<12 ND ND ND NA 0 5 <br /> t-Butyl alcohol(TBA) ND<120 ND ND ND NA 5 0 <br /> Dtvsopropyl ether(DIPE) ND<12 ND ND ND NA 0 5 <br /> Ethylbenzene ND<12 ND ND ND NA 0 5 <br /> Ethyl tert-butyl ether(ETRE) ND<12 ND ND ND NA 05 <br /> Methyl-t-butyl ether(MTBE) 690 ND 12 0 82 NA 0 5 <br /> ' Toluene ND<12 ND ND ND NA 0 5 <br /> Xylenes ND<12 ND ND ND NA 05 <br /> 1 Surrogate Recoveries(%) <br /> %SS 92 7 97 8 961 948 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soll/sludge/sohd samples in gg/kg, wipe samples inµgtwtpe, <br /> ' product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> h)lighter than water tmmtsctble sheen/product is present,t)liquid sample that contains greater than—2 vol %sediment,3)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />