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t 10 2nd Avenue South #1137 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-,620 Fax 925-798.1622 <br /> http//www mecanipbell com E-niad mam(&)naccampbell com <br /> Advanced GeoEnvironmental, Inc Client Project ID Country Club Food& Date Sampled 08/12/02 <br /> Fuel <br /> 837 Shaw Road Date Received 08/13/02 <br /> Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 08/17102-08/19/02 <br /> ' Client P O Date Analyzed 08/17/02-08/19/02 <br /> Oxygenates and BTEX by GC/MS* <br /> Extrac11011 Method SW5030B Analytical Method SW8260B Work Order 0208188 <br /> ' Lab 1D 0208188-OO1C 0208188-002C 0208188-003C j 0208188-004C <br /> Client 1D M W i/08-12-02 M W2/08-1 2-02 M W3/08-12-02 M W4/08-12-02 <br /> Reporting Limit for <br /> Matrix W W W W DF=l <br /> ' Compound Concentration ug/kg pg/L <br /> tert-Amyl methyl ether(TAME) ND<20 ND ND ND NA 05 <br /> Benzene ND<20 ND ND ND NA 05 <br /> t-Butyl alcohol(TBA) ND<200 ND ND ND NA 50 <br /> Diisopropyl ether(D1PE) ND<20 ND ND ND NA 05 <br /> Fthylbenzene ND<20 ND ND ND NA 05 <br /> Ethyl tel t-butyl ether(ETBE) ND<20 ND ND ND NA 05 <br /> ' Methyl-t-butyl ether(MTBE) 480 ND 12 1 I NA 05 <br /> Toluene mm ND<20 ND ND ND NA 05 <br /> Xyleites ND<20 ND ND ND NA 05 <br /> Surrogate Recoveries(%) <br /> %SS�— --- - 995 - 981 s � 975 5 - - �07 6--� <br /> ' Comments <br /> -- <br /> *watei and vapor samples and all TCLP&SPLP exti acts are reported in ug/L,soil/sludge/solid samples in ug/kg, wipe samples in uglwipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> ' h)lighter than water immiscible sheen/product is present i)liquid sample that contains greater than--2 vol %sediment,j)sample dilated due to high <br /> organic content <br /> 1 <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />