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Report Number 31263 QC Report Matrix Spike/Matrix Spike Duplicate Date 2110/2003 Project Name SANCHEZ Project Number Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 31263-14 32 400 397 66 7 654 ug/L EPA 82606 217103 864 839 2 95 70-130 25 Toluene 31263-14 24 400 397 583 572 uglL EPA 82608 217103 867 846 245 70-130 25 Tert-Butanol 31263-14 <5 0 200 198 189 188 uglL EPA 8260B 217103 944 950 0 586 70-130 25 Methyl-t-Butyl Ether 31263-14 21 400 397 623 620 uglL EPA 82608 217103 104 104 00635 70-130 25 Benzene 31277-17 <0 50 400 400 423 401 uglL EPA 82608 215103 106 100 517 70-130 25 Toluene 31277-17 <0 50 400 400 38 2 361 uglL EPA 8260B 215103 95 4 902 560 70-130 25 Tert-Butanol 31277-17 <5 0 200 200 212 206 uglL EPA 8260E 215103 106 103 286 70-130 25 Methyl-t-Butyl Ether 31277-17 <0 50 400 400 41 1 427 ug/L EPA 8260B 215103 103 107 365 70-130 25 Benzene 31248-01 <0 50 400 400 370 354 uglL EPA 8260B 213103 92 4 885 4 34 70-130 25 Toluene 31248-01 <0 50 400 400 35 8 35 7 ug[L EPA 62608 213103 89 4 892 0 224 70-130 25 Tert-Butanol 31248-01 51 200 200 244 276 ug/L EPA 82606 213103 964 112 152 70-130 25 Methyl-t-Butyl Ether 31248-01 12 400 400 518 51 1 uglL EPA 8260E 213!03 996 980 167 70-130 25 Benzene 31246-01 <0 50 400 400 39 7 384 ug/L EPA 8260E 214!03 99 2 961 322 70-130 25 Toluene 31246-01 <0 50 400 400 368 335 uglL EPA 8260B 2!4103 920 838 930 70-130 25 Tert-Butanol 31246-01 <5 0 200 200 195 185 uglL EPA 8260B 214103 974 923 536 70-130 25 Methyl-t-Butyl Ether 31246-01 <0 50 400 400 41 5 41 0 uglL EPA 8260B 214103 104 102 126 70-130 25 Benzene 31357-01 <0 50 400 400 41 7 41 0 uglL EPA 8260B 217103 104 102 172 70-130 25 Toluene 31357-01 <0 50 40 0 400 382 37 1 uglL EPA 8260B 2!7103 95 6 928 305 70-130 25 Approved By J el Kiff KIFF ANALYTICAL, LLC S 1i 2795 2nd Sl, Suite 300 Davis,CA 95616 530-297-4800 V