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Report Number 34398 4C Report Matrix Spike!Matrix Spike Duplicate Date 8/1112003 Protect Name SANCHEZ 114 LY Protect Number Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff —--_ ParameterSample_ Value Level eve! Value Value Units Method ....Analyzed Recov Recov Diff Limit Limit Benzene 34394-03 21 394 400 598 605 ug/L. EPA 8260E 818103 981 9132 0 152 70-130 25 Toluene 34394-03 12 394 400 532 54 0 ug/L. EPA 8260B 818103 104 104 0 179 70-130 25 Tert-Butanol 34394-03 11 197 200 190 199 ug/L. EPA 82608 818103 908 939 334 70-130 25 Methyl-t-Butyl Ether 34394-03 40 394 400 80 9 768 ugiL EPA 82608 818103 103 908 123 70-130 25 Benzene 34395-01 <0 50 400 400 399 39 6 ugiL EPA 8260B 818103 998 990 0 830 70-130 25 Toluene 34395-01 <0 50 400 400 437 428 ugiL EPA 8260B 818103 109 107 2 06 70-130 25 Tert-Butanol 34395-01 <50 200 200 203 203 ugiL EPA 82608 818/03 101 102 0 271 70-130 25 Methyl-t-Butyl Ether 34395-01 <0 50 400 400 427 427 ug/L EPA 82606 8/8/03 107 107 0117 70-130 25 Benzene 34398-08 <0 50 400 400 39 7 389 ug/L EPA 8260E 819103 992 972 2 09 70-130 25 Toluene 34398-08 <0 50 400 400 427 422 ugiL EPA 8260B 819/03 107 106 120 70-130 25 Tert-Butanol 34398-08 <5 0 200 200 202 201 ug/L EPA 8260B 819/03 101 100 0 670 70-130 25 Methyl-t-Butyl Ether 34398-08 <0 50 400 400 436 408 ugiL EPA 82608 819103 109 102 673 70-130 25 Benzene 34398-04 <0 50 400 400 403 400 ug/L EPA 8260E 819/03 101 999 0 897 70-130 25 Toluene 34398-04 <0 50 400 400 467 45 7 ugiL EPA 8260B 819103 117 114 223 70-130 25 Tent-Butanol 34398-04 <50 200 200 203 199 ugiL EPA 8260B 819103 101 993 1 97 70-130 25 Methyl-t-Butyl Ether 34398-04 <0 50 400 400 35 5 35 6 ugiL EPA 8260B 819103 888 890 0 309 70-130 25 Approved 8y KIFF ANALYTICAL, LLC / 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800 i