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I Report Number 367�11 QC Report Matrix Spike/Matrix Spike Duplicate Date 1/22/2004 Protect dame Sanchez Protect Number Duplicate Duplicate Spiked p Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Analyzed Percent Percent aSample Spike eDeSample Sample Analysis $ Dvt t centLivLParameter Sample VLel Level Value Units Method ReoRecov Percent Limit Benzene 36500-04 <0 50 400 400 39 3 38 6 ug/L EPA 82608 1119104 982 966 159 70-130 25 Toluene 36500-04 <0 50 400 400 39 9 393 ug/L EPA 82606 1119104 996 983 1 34 70-130 25 Tert-Butanol 36500-04 <5 0 200 200 190 188 ug/L. EPA 8260B 1119104 949 938 1 14 70-130 25 Methyl-t-Butyl Ether 36500-04 <0 50 400 400 416 41 7 ug/L EPA 8260B 1119104 104 104 00961 70-130 25 I Benzene 36711-03 <0 50 400 400 473 474 ug/L EPA 8260B 1117/04 118 118 0 254 70-1301 25 Toluene 36711-03 <0 50 400 400 458 46 0 ug/L EPA 8260B 1/17/04 114 115 0 479 70-130 25 Tert-Butanol 36711-03 <5 0 200 200 209 207 ug/L EPA 82606 1/17/04 105 104 0 998 70-130 25 Methyl-t-Butyl Ether 36711-03 <0 50 400 400 40 3 406 ug/L EPA 82608 1/17/04 101 102 0 741 70-1301 25 Benzene 36707-01 <0 50 400 400 473 469 ug/L EPA 82608 1/17/04 118 117 0 786 70-930 ; 25 Toluene 36707-01 <0 50 400 400 462 460 ug/L. EPA 82606 1/17104 116 115 0 564 70-130 25 Tert-Butanol 36707-01 <5 0 200 200 207 202 ug/L EPA 8260B 1/17/04 103 101 260 70-1301 25 Methyl-t-Butyl Ether 36707-01 <0 50 400 400 427 429 ug/L EPA 8260B 1/17104 107 107 0 468 70-130 f 25 Benzene 36734-06 <0 50 400 400 409 400 ug/L EPA 8260E 1/22//04 102 999 225 70-130 25 Toluene 36734-06 <0 50 400 400 356 362 ug/L EPA 8260B 1/22/04 890 906 167 70-130 � 25 Tert-Butanol 36734-06 <5 0 200 200 192 191 ug/L EPA 82606 1/22/04 95 8 956 0 214 70-130 25 Methyl-t-Butyl Ether 36734-06 85 400 400 476 459 ug/L EPA 82606 1/22104 978 934 463 70-130 l 25 I 1 Approved By i J &I VI KIFF ANALYTICAL, LLC ' 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800