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819 Striker Avenue, Suite 8 <br /> Sequoia Sacramento, 92 9583 <br /> 92 4 <br /> {916) 1-9600 <br /> ® FAX(916)921-0100 <br /> 1 nalytica� www.sequoialabs.com <br /> Upgradient-Valley Springs Project: Kwikee Foods <br /> Reported: <br /> 336 Augusta Court Project Number: NIA <br /> Project Manager: Vic Cherven 01/02/01 14:44 <br /> Valley Springs CA,95252 <br /> Volatile Oxygenate Compounds by TEPA Method 8260A - Quality Control <br /> Sequoia Analytical - Sacramento <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit units Level Result %REC Limits RPD Limit Motes <br /> Batch 0120228-PPA 5030B [PIT) <br /> Blank(0120228-BLKI) _ _ .- _ Prepared&Analyzed: 12/19/00 <br /> -Cert-butyl alcohol ND 200 ug/l <br /> Methyl tert-butyl ether ND 2.00 <br /> Di-isopropyl ether ND 2.00 " <br /> Ethyl tert-butyl ether ND 2.00 <br /> `Cert-amyl methyl ether ND 2.00 <br /> Ethanol ND 3000 -- - —— -— ---- - --- - <br /> - - - ---- 48.0 - -- —--- 50.0 96.0 60-140 <br /> Surrogate: 1,2-DCA-d4 <br /> LCS(0120228-SS1) _ _ __ _ _-__ _— _ Prepared&Analyzed: 12/19/00 <br /> 53.8 2.00 ug/t 50.0 108 70-130 <br /> Methyl ter(-butyl ether - - -- - _ <br /> 50.0 105 60-140 <br /> Surrogate: 1,2-DCA-d4 <br /> -52 6 <br /> Dup(0120228-BSD1) _ _ - - Prepared&Analyzed: 12119100- - <br /> ethyl tert-butyl ether 57.4 — — 2.00 u9'1 1 50.0 115 70-130 6.47 200 <br /> - - -54.0 11 50.0 108 60-140 <br /> Surrogate: 1,2-DCA-d4 <br /> Matrix Spike(0120228-MSS) - _— _Source: 5012140-10 - _ Prepared&Analyzed_ 12119/00- <br /> Methyl Cert-butyl ether 55.8 -- 2.00 _ ug/I — 50_0^ ND 112 60-I40 - <br /> - -- ---- — 53.2 50.0 106 60-140 <br /> surrogate: 1,2-DCA-d4 <br /> Matrix Spike Dup(0120228-MSDI) Source: 5012140-110 Prepared&Analyzed_ 12/19/00 <br /> ---- <br /> Methyl tert-butyl ether 52.6 2.00 — ugll 50.0 ND 105 60-140 5.90 25 <br /> Surrogate: 1,2-DCA-d4 <br /> -- — — 51.8— 1150.0 104 60-140 <br /> gttoia Analytical - Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document. This analytical report must be reproduced in its entirety. <br /> Page 7 of 9 <br />