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0 0 Report Number 4015 QC Report • Matrix Spike/Matrix Spike Duplicate Date 5/20/2005 Project Name 2575 Country Club Project Number 247-0783-003 Duplicate Spiked Duplicate Spiked Spiked Sample Relative Spike Spiked Spiked Sample Sample Relative Percent Percent Spiked Sample Spike Dup Sample Sample Analysis Date Percent Percent Percent Recov Diff Parameter Sample Value Level Level Value Value Units Method Analyzed Recov Recov Diff Limit Limit Benzene 43792-03 7 0 39 8 394 51 8 51 5 ug/L EPA 82606 5119105 113 113 00730 70-130 25 Toluene 43792-03 1 8 398 394 460 45 0 ug/L EPA 8260B 5119105 111 109 146 70-130 25 Tert-Butanol 43792-03 <5 0 199 197 203 196 ug/L EPA 8260B 5119105 102 995 272 70-130 25 Methyl-t-Butyl Ether43792-03 <0 50 398 394 409 418 ug/L EPA 8260B 5119105 103 106 312 70-130 25 Benzene 43831-01 <0 50 400 400 423 409 ug/L EPA 82606 5118105 106 102 334 70-130 25 Toluene 43831-01 <0 50 400 400 410 397 ug/L EPA 8260B 5118105 102 992 333 70-130 25 Tert-Butanol 43831-01 <5 0 200 200 182 203 ug/L EPA 8260B 5118105 909 101 109 70-130 25 Methyl-t-Butyl Ether43831-01 <0 50 400 400 359 35 3 uglL EPA 82608 5118105 89 8 88 3 162 70-130 25 Benzene 43795-02 32 400 400 734 721 ug/L EPA 82606 5117105 103 99 7 308 70-130 25 Toluene 43795-02 21 400 400 627 615 ug/L EPA 82606 5/17105 103 100 299 70-130 25 Tert-Butanol 43795-02 1000 200 200 1200 1230 ug/L EPA 8260B 5117105 978 111 128 70-130 25 Methyl-t-Butyl Ether43795-02 140 400 400 184 184 ug/L EPA 8260B 5117105 101 101 0 432 70-130 25 Benzene 43808-08 <0 50 400 400 416 409 ug/L EPA 8260B 5119105 104 102 160 70-130 25 Toluene 43808-08 <0 50 400 400 412 410 uglL EPA 8260B 5/19105 103 102 0 679 70-130 25 Tert-Butanol 43808-08 <50 200 200 202 204 ug1L EPA 8260B 5119105 101 102 123 70-130 25 Methyl-t-Butyl Ether 43808-08 <0 50 400 400 400 398 ug/L EPA 8260B 5119105 100 996 0 512 70-130 25 KIFF ANALYTICAL, LLC Approved By Jo I Iff 2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800