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885 larAs Drive <br /> Sequoia morgan(07'6- <br /> 4 4 FAX(408)782-6308 <br /> _ Analytical VVWW SeqLxAahIbS COM <br /> Blaine Tech Services(Shell) Project 2575 Country Club <br /> 1680 Rogers Avenue Project Number 2575 Country Club/Stockton Reported <br /> San Jose CA,95112 Project Manager Nick Sudano 08/14/00 17 58 <br /> Volatile Organic Compounds by EPA Method 8260A - Quality Control <br /> Sequoia Analytical- Morgan Hill <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 0H14011 -EPA 5030B [PIT] <br /> LCS(OH 14011-BSI) Prepared&Analyzed 08/12/00 _ <br /> Methyl tert-butyl ether 100 100 uglt 100 100 70-130 <br /> Surrogate 1 2-Dichloroethane-d4 975 100 975 70-130 <br /> Batch OH14030-EPA 5030B PIT <br /> Blank(OH14030-BLK1) _ _ Prepared&Analyzed 08/14/00 <br /> Ethanol ND 400 ugA <br /> ten-Butyl alcohol ND 200 <br /> Methyl tert-butyl ether ND too " <br /> Di-isopropyl ether ND 100 " <br /> Ethyl tert-butyl ether ND 1000 " <br /> Amyl methyl ether ND 100 " <br /> -Dichloroethane ND 100 " <br /> Ethylene dibromide ND too " <br /> Surrogate 1 1-Dichloroethane-d4 811 100 821 70430 ' <br /> LCS(OH14030-BS I) T _ _ Prepared&Analyzed 08/14/00 <br /> Methyl tert-butyl ether 979 100 ug/1 t 0 0 879 70-130 <br /> Surrogate 12-Dichloroethane-d4 872 100 872 70-130 <br /> Matrix Spike(01114030-MS1) Source MJH0016-01 Prepared&Analyzed 08/14/00 <br /> Methyl tert-butyl ether 1710 100 ug/l 1000 171 70-130 <br /> Surrogate 1 2-Drchloroethane-d4 739 100 739 70-130 <br /> Matnx Spike Dup(OH14030-MSDI) Source MJH0016-01 Prepared&Analyzed 08/14/00 <br /> Methyl tent-butyl ether 1800 loo ug/l 1000 180 70-I30 5 13 25 <br /> Surrogate 11-Dichloroethane-d4 886 100 886 70-130 <br /> quoia Analytical-Morgan Hill Tice results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document This analytical report must be reproduced in its entirety <br /> Page 23 of 24 <br />